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Method of extracting soyabean isoflavone and soya bean saponin for soya bean whey waste water

A technology of soybean whey wastewater and soybean isoflavones, which is applied in chemical instruments and methods, preparation of sugar derivatives, sugar derivatives, etc., can solve the problems of single material recovery, complex process, high cost, etc., and achieve simple process and broad market Prospect, low cost effect

Inactive Publication Date: 2006-11-01
TONGFANG ENVIRONMENT
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Problems solved by technology

The Chinese patent has published an invention patent of "a process for extracting soybean isoflavones and soybean saponins" with application number 00105542, which introduces the use of high-temperature flash evaporation, electrodialysis and cationic resin exchange in the whey discharged from the production of soybean protein isolate and non-polar macroporous resin adsorption and elution technology to obtain soybean isoflavones and soybean saponins, but this method has the problems of complex process, single material recovery, and high cost

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  • Method of extracting soyabean isoflavone and soya bean saponin for soya bean whey waste water
  • Method of extracting soyabean isoflavone and soya bean saponin for soya bean whey waste water
  • Method of extracting soyabean isoflavone and soya bean saponin for soya bean whey waste water

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Effect test

Embodiment 1

[0038] Embodiment one, refer to figure 1 :

[0039] ① Pretreatment:

[0040] a) Put the soybean whey wastewater obtained by producing soybean protein isolate by one-step alkali-dissolving and acid-precipitating process into a flocculation tank, and carry out flocculation and centrifugation by adjusting the pH value and adding electrolytes. b) Filtrating the flocculation centrifugate through a bag filter and a microfilter to obtain a microfiltration permeate A1. c) concentrating the microfiltration permeate A1 through an ultrafiltration device to obtain ultrafiltration permeate B1 and ultrafiltration concentrate C1.

[0041] ②Resin series adsorption recovery of soybean isoflavones and soybean saponins:

[0042] a) The ultrafiltration permeate B1 is passed through the series resin column of different weakly polar macroporous adsorption resin columns X1 and X2 at a flow rate of 1.5BV / h to obtain the effluent D1, wherein the volume of the ultrafiltration permeate B1 is equal to...

Embodiment 2

[0049] Embodiment two, refer to figure 2 :

[0050] ① Pretreatment:

[0051] a) Put the soybean whey wastewater obtained by producing soybean protein isolate by one-step alkali-dissolving and acid-precipitating process into a flocculation tank, and carry out flocculation and centrifugation by adjusting the pH value and adding electrolytes. b) Filtrating the flocculation centrifugate through a bag filter and a microfilter to obtain a microfiltration permeate A2. c) concentrating the microfiltration permeate A2 through an ultrafiltration device to obtain ultrafiltration permeate B2 and ultrafiltration concentrate C2. d) Concentrating the ultrafiltration permeate B2 through a nanofiltration device to obtain nanofiltration permeate N-F and nanofiltration concentrate D-C.

[0052] ②Resin series adsorption recovery of soybean isoflavones and soybean saponins:

[0053] a) Add pure water equivalent to twice its volume to the nanofiltration concentrated solution D-C to obtain the ...

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Abstract

A method for extracting soybean isoflavones and soybean saponins from soybean whey wastewater relates to the technical fields of soybean deep processing and wastewater resource utilization. The method is as follows: adjust the pH value of the soybean processing wastewater, centrifuge, pre-filter and micro-filter and other pretreatments; then use resin series adsorption to recover soybean isoflavones and soybean saponins; then separate soybean isoflavones and soybean saponins; and then extract primary soybeans Saponin products; obtain high-purity soybean saponin products. Experiments have proved that the soybean isoflavone and soybean saponin products obtained by using the method can meet market requirements. The process of the present invention is simple, and the required equipments are common devices in the soybean deep processing industry and water treatment industry. The weakly polar macroporous adsorption resin used is also a commercially available product, with low cost, very easy to popularize, beneficial to large-scale production, and has broad application potential. market prospects. Simultaneously, the invention further controls the pollution of soybean whey wastewater, and has remarkable economic, environmental and social benefits.

Description

technical field [0001] The invention relates to the technical field of soybean deep processing and wastewater resource utilization, in particular to a method for extracting soybean isoflavones and soybean saponins from soybean whey wastewater. Background technique [0002] At present, the production of soybean protein isolate in China mainly adopts the traditional alkali-soluble acid precipitation process, which discharges about 40-70m3 per ton of soybean protein isolate. 3 Soy whey wastewater, its COD Cr The general range of 15000 ~ 30000mg / L. In the prior art, most of the treatment of soybean whey wastewater is anaerobic-aerobic biological treatment process. This traditional process can generally remove the COD in soybean whey wastewater. Cr Remove 80-90%. However, the treatment effect of this biological treatment process is unstable, and is often restricted by various objective factors such as wastewater quality and seasonal changes. At the same time, the investment co...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07D311/36C07H17/075C07H1/06
Inventor 王占生朱翠萍
Owner TONGFANG ENVIRONMENT
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