Protein synthetic fiber and its production method
A technology of synthetic fibers and manufacturing methods, applied in the direction of cellulose/protein conjugated artificial filaments, etc., can solve problems such as trouble, inability to guarantee fiber quality, protein loss, etc., achieve good air permeability and moisture conductivity, simple and easy preparation, increase The effect of miscibility
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Embodiment 1
[0023] Example 1: Add soybeans that have been soaked in water and wet ground into an alkaline solution with a pH of 9.6, and dissolved at a temperature of 29°C. The ratio of material to water is 1:15, and the dissolution time is 180 minutes. Gelatin is added to an alkaline solution with a pH of 9.6, and dissolved at a temperature of 28°C. The ratio of material to water is 1:40. The dissolution process is 240 minutes. The dissolution process should be stirred, and then stand still to separate and remove the waste residue. To obtain the extract, add hydrochloric acid to the extract to adjust the isoelectric point of the extract to obtain the isolated protein; the obtained plant isolated protein and animal isolated protein are dissolved in a triethanolamine-containing pH 12 with a dry solid weight ratio of 1:29 In the aqueous solution, the initial temperature of dissolution is 30°C and then heated to 91°C, and then the temperature is raised to 95°C, and kept at 95°C for 20 minutes to...
Embodiment 2
[0025] Example 2: Put the crushed and defatted soybeans and cheese protein into a solution with a pH of 7.8, and dissolve them at a temperature of 28°C. The dissolution time is 120 minutes. The dissolution process should be stirred and then left to stand. Separate and remove the waste residue to obtain the leachate. Add phosphoric acid to the leachate to adjust the isoelectric point to obtain the separated protein. The two separated proteins are dissolved in a solution containing triethanolamine with a pH of 1.5 at a ratio of 5:21. The temperature is 40°C, and then heated to 95°C and kept at 95°C for 20 minutes to prepare a protein solution with an As concentration of 5%; add the washed polyvinyl alcohol (PVA) into the protein solution, Blend and copolymerize at a temperature of 95°C, raise the temperature to 98°C and keep for 60 minutes to prepare a spinning solution containing animal and plant proteins and polyvinyl alcohol, and adjust the solution to a concentration of 10%, and...
Embodiment 3
[0027] Example 3: Put the defatted cottonseed meal into a solution with a pH of 9.5, and dissolve it at a temperature of 29.5°C. The ratio of material to water is 1:15, and the dissolution time is 70 minutes. The dissolution process should be stirred. Then let it stand to separate and remove the waste residue to obtain the leachate. Add phosphoric acid to the leachate to adjust the isoelectric point to obtain the plant protein separation. Add shellac to an alkaline solution with a pH of 10. The ratio of material to water is 1:15. Dissolve under the condition of 29.5℃, the dissolution time is 100 minutes, the dissolution process should be stirred, and then stand still to separate and remove the waste residue to obtain the leachate. Add phosphoric acid to the leachate to adjust the isoelectric point of the leachate to obtain animal separation protein; separate the plant Protein and animal separated protein were dissolved in a solution containing triethanolamine with a pH of 3 at a r...
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