Nano rare earth m-hydroxy benzoic acid 8-hydroxyquinoline antibacterial agent and method for preparing same
A technology of hydroxybenzoic acid and hydroxybenzoquinoline, applied in the field of antibacterial agents, can solve the problems of affecting the appearance of white or light-colored products, use restrictions, and high prices, achieve high chemical stability and thermal stability, and reduce prices and costs. low effect
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[0008] The preparation method of the present invention is to get 0.01mol sodium m-hydroxybenzoate and mix it with 0.02mol 8-hydroxyquinoline in a magnetic stirrer to obtain a mixed ligand solution; at a temperature of 40°C, drop this mixed ligand solution into to 0.01mol RECl 3 6H 2 In O, adjust the pH value=more than 6, react for 2 hours, and age for 0.5 hour; filter with sand core funnel, then wash with double distilled water to remove chloride ion (Cl - ) was dried under vacuum for 4 hours to obtain RE(MBA)(hq) 2 Rare earth m-hydroxybenzoic acid 8-hydroxyquinoline; finely ground, measured, bottled and placed in a desiccator.
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