Supersonic liquid phase reduction process for preparing monodisperse nano germanium crystal
A monodisperse and nanocrystalline technology, which is applied in the field of ultrasonic liquid phase reduction to prepare monodisperse germanium nanocrystals, can solve the problems of uneven particle size distribution, high cost, and harsh conditions for nanocrystalline materials, and achieve low cost and high conditions. Effects that are not harsh and the preparation method is simple
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Embodiment 1
[0032] According to the preparation process, the specific GeCl 4 Amount of 10ml 0.01mol / l THF solution, such as figure 1 The reducing agent shown in (a) is NaBH 4 10ml of 0.06mol / l ethanol solution; figure 1 The reducing agent shown in (b) is LiAlH 4 The consumption is the THF solution of 10ml 0.06mol / l; figure 1 (c) The reducing agent is 85% N 2 h 4 h 2 O solution 1ml. All the reactions were performed under the action of ultrasonic waves with an ultrasonic frequency of 40KHz for 30 minutes.
Embodiment 2
[0034] figure 2 (a) The sample is carried out according to the preparation process, using specific GeCl 4 The amount is 10ml of 0.01mol / l THF solution, using reducing agent NaBH 4 The dosage is 10ml of 0.06mol / l ethanol solution. The reaction was performed under the action of ultrasonic waves with an ultrasonic frequency of 50KHz for 30 minutes. figure 2 The reaction of (b) sample is carried out in the process of magnetic stirring at a stirring rate of 300r / min, using specific GeCl 4 The amount is 10ml of 0.01mol / l THF solution, and the reducing agent is NaBH 4 The specific dosage is 10 ml of 0.06 mol / l ethanol solution, and the reaction time is 30 minutes.
Embodiment 3
[0036] image 3 (a) The sample is carried out according to the preparation process, using specific GeCl 4 Amount of 10ml 0.01mol / l THF solution, reducing agent NaBH 4 The specific dosage is 10ml of 0.06mol / l ethanol solution. image 3 (b) using specific GeCl 4 The amount is 10ml of 0.1mol / l THF solution, and the reducing agent is NaBH 4 The specific dosage is 10ml of 0.6mol / l ethanol solution. All reactions were performed under ultrasound for 30 minutes.
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