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Method for preparing solution for controlling cucumber and tomato disease using albizzia julibrissin extract

An extract and the technology of using Albizia julienne, applied in the field of pesticides, can solve the problems of no research reports on the prevention and treatment of plant diseases by leaves of Albizia julienne, no research on leaf extracts, etc., and achieve the effects of easy artificial cultivation, good preventive effect, and simple extraction process

Inactive Publication Date: 2005-12-21
SHANGHAI JIAO TONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] After searching the existing technical literature, it was found that Zhao Boguang published an article in the "Journal of Nanjing Forestry University" (Volume 18, No. 2) entitled: "The antifeeding effect and toxicity of six plant extracts on Pinus massoniana caterpillars" It is reported in the article that the bark extract of Albizia Julibrissin has an antifeedant effect on the larvae of Pinus massoniana caterpillars. The bark of Albizia Julibrissin is used as the raw material, and it is first extracted and degreased by petroleum ether (30-60°C) with a Soxhlet fat extractor. Finally, 95% analytical pure ethanol was used to extract the ethanol extract, but no research was carried out on the leaf extract of Albizia Julibrissin; in further searches, no research reports on the use of leaves of Albizia Julibrissin in preventing and controlling plant diseases were found.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] The weight percent of water agent for controlling cucumber and tomato diseases: 0.95% of Albizia Julibrissin leaf extract, 99.05% of distilled water.

[0014] Weigh 20 g of Albizia Julibrissin leaf powder (20 mesh particles), immerse and extract 3 times with 200 ml of 95% ethanol at room temperature, each time for 24 hours, concentrate under reduced pressure and recover the solvent to obtain 3.1 g of dry matter; use ultrasonic waves to suspend the dry matter with 50 ml of water, Equal volumes of petroleum ether, ethyl acetate, and water-saturated n-butanol were extracted 5 times in sequence, and the n-butanol phase extract was concentrated to obtain 0.95 g of the extract, which was dissolved in 100 ml of water and filtered to prepare a water solution with a concentration of 0.95%. ; The indoor preventive test on cucumber downy mildew was carried out by using the leaf disk floating method, and the control effect on cucumber downy mildew reached 88.89%.

Embodiment 2

[0016] The weight percent of water agent for controlling cucumber and tomato diseases: 3% of Albizia Julibrissin leaf extract, 97% of distilled water.

[0017] Weigh 40g of Albizia Julibrissin leaf powder (20 mesh particles), soak and extract 3 times with 400ml of anhydrous methanol at room temperature, each time for 24 hours, concentrate under reduced pressure and recover the solvent to obtain 10.3g of dry matter; use ultrasonic waves to suspend the dry matter with 100ml of water, An equal volume of petroleum ether, ethyl acetate, and water-saturated n-butanol were extracted 5 times in sequence, and the n-butanol phase extract was concentrated to obtain 1.9 g of the extract, which was dissolved in 63.33 ml of water, filtered, and prepared into a 3% Water agent; the indoor pot test is used to carry out the preventive test on cucumber downy mildew, and its control effect reaches 62.00%.

Embodiment 3

[0019] The weight percent of water agent for controlling cucumber and tomato diseases: 0.95% of Albizia Julibrissin leaf extract, 99.05% of water.

[0020] Weigh 40g of Albizia Julibrissin leaf powder (20 mesh particles), soak and extract 3 times with 400ml of anhydrous methanol at room temperature, each time for 24 hours, concentrate under reduced pressure and recover the solvent to obtain 10.3g of dry matter; use ultrasonic waves to suspend the dry matter with 100ml of water, An equal volume of petroleum ether, ethyl acetate, and water-saturated n-butanol were extracted 5 times in sequence, and the n-butanol phase extract was concentrated to obtain 1.9 g of the extract. The extract was dissolved in 200 ml of water, filtered, and prepared into a water solution with a concentration of 0.95%. agent; using Tianwen district test to prevent cucumber downy mildew, its control effect reached 48.84%. The control effect is significantly different from that of the blank control (sprayi...

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PUM

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Abstract

The present invention relates to a preparation method of silk tree leaf extract aqueous preparation for controlling diseases of cucumber and tomato. Said preparation method mainly includes the following steps: collecting fresh silk tree leaf, drying, pulverizing to obtain powder, using absolute methyl alcohol as extraction solvent, soaking said silk tree leaf powder to make extraction, reduced pressure concentrating the extract to obtain silk tree leaf paste, adding said silk tree leaf paste into distilled water, then placing them in ultrasonic wave generator to make the dried material be suspended, successively using petroleum ether, ethyl acetate and water saturated normal butanol to make respective extraction for 5 times, concentrating the extract and drying to obtain silk tree leaf extract, and dissolving said extract by water so as to obtain the invented product with good effect for preventing downy mildew of cucumber and grey mould of tomato.

Description

technical field [0001] The invention relates to a preparation method in the technical field of pesticides, in particular to a method for preparing water agents for controlling cucumber and tomato diseases by using Albizia Julibrissin extract. Background technique [0002] Cucumber and tomato are the main vegetable varieties loved by the public. Cucumber downy mildew and tomato gray mold are important fungal diseases that have plagued vegetable cultivation, especially facility cultivation in recent years. Generally, the yield can be reduced by 10%-20%. Reduce production by more than 50%. At present, chemical pesticides are generally used to control such diseases, and it has become a consensus on the harm caused by chemical pesticides to the environment and human health, and the resistance of the controlled objects. The purpose of the invention of this patent is to control the occurrence of these two diseases by using the water preparation prepared from the natural non-toxic ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N65/20
Inventor 代光辉赵杰陈晓斌顾振芳
Owner SHANGHAI JIAO TONG UNIV
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