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Apparatus and method for recovering carbon disulfide in hydrogen sulfide gas during preparing process of carbon disulfide

A technology of carbon disulfide and hydrogen sulfide, which is applied in the field of separation of gas mixtures, can solve problems such as environmental pollution, economic loss, and reduction of catalyst activity, and achieve the effects of protecting the environment, reducing the concentration of sulfur dioxide, and increasing the concentration of acid gas

Inactive Publication Date: 2007-02-28
孔庆然
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Problems solved by technology

[0003] In order to solve the problem that the hydrogen sulfide gas containing carbon disulfide separated in the existing carbon disulfide production process directly enters the Claus recovery system, it not only causes certain economic losses, but also reduces the activity of the catalyst in the Claus reactor and pollutes the environment, etc. To solve the problem and provide a kind of equipment and method for recovering carbon disulfide in hydrogen sulfide gas in the preparation of carbon disulfide

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  • Apparatus and method for recovering carbon disulfide in hydrogen sulfide gas during preparing process of carbon disulfide

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Embodiment Construction

[0011] The equipment for recovering carbon disulfide in hydrogen sulfide gas in the preparation of carbon disulfide includes at least two adsorption reactors. The mixed gas input branch pipe 8 connected with the mixed gas input main pipe 7 is respectively connected under the adsorption reactor. The carbon disulfide output branch pipe 9 communicated with the gas input branch pipe 8, the carbon disulfide output branch pipe 9 is connected with the vacuum desorption pump 5 respectively, the hydrogen sulfide output pipe 10 is respectively arranged above the adsorption reactor, and valves are respectively installed on each pipe; There is also an adsorption buffer tank 4 between the desorption pumps 5, and the top of the adsorption buffer tank 4 is respectively connected to the hydrogen sulfide output pipe 10 and the vacuum desorption pump 5 through a vacuum pipeline 12; preprocessor6.

[0012] Utilize the above-mentioned equipment for recovering carbon disulfide in hydrogen sulfide ...

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Abstract

The invention discloses a recycling equipment and method of carbon disulfide in the hydrogen sulfide, which is characterized by the following: injecting hydrogen sulfide with carbon disulfide in the Claus recycling system directly; maintaining inner catalyst active property in the Claus reactor; sending the hydrogen sulfide with carbon disulfide in the adsorbing reactor to proceed adsorb and desorb operations alternately; transmitting the desorbed carbon disulfide in the refining unit to recycle carbon disulfide.

Description

technical field [0001] The invention relates to a separation method of a gas mixture, in particular to a device and a method for recovering carbon disulfide in hydrogen sulfide gas during the preparation of carbon disulfide. Background technique [0002] At present, during the preparation of carbon disulfide, the mixture of sulfur, carbon disulfide and hydrogen sulfide (process gas) from the reactor enters the preliminary separation tower for separation, and the unreacted sulfur is discharged from the bottom of the tower, while the mixed gas of carbon disulfide and hydrogen sulfide is produced by The top of the tower is discharged and cooled, wherein the condensed carbon disulfide is refluxed to the separation tower for washing and cooling the residual sulfur, and the hydrogen sulfide gas with about 0.5-8% carbon disulfide is directly discharged to the Claus tail gas recovery system, like this, On the one hand, part of the finished product of carbon disulfide was converted i...

Claims

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Application Information

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IPC IPC(8): C01B31/26
Inventor 孔庆然
Owner 孔庆然
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