Skin Penetration Enhancing Systems for Polar Drugs
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example 1
In Vitro Percutaneous Absorption of 2,5-Dihydroxybenzenesulfonate from Various Formulations
Methods
[0162]An in vitro percutaneous absorption study evaluated tissue permeation and penetration of 2,5-dihydroxybenzenesulfonate from various formulations along with controls 10% Calcium Dobesilate in DMSO and Doxiproct® Ointment (4% Calcium Dobesilate). The composition of the formulations evaluated in this study is summarized below.
Formulations:
[0163]A. ID: 2567-20A (Calcium Dobesilate, 10% in DMSO). DMSO is known to provide the maximum skin permeability of many pharmaceutical ingredients.
B. ID: Doxiproct® Ointment (4% Calcium Dobesilate, Lot# OM Portuguesa, S.A. 151065) PEG (polyethylene glycol) Base ointment. Commercially available for the treatment of hemorrhoids.
C. ID: 2567-19B (Cream, 5% Potassium 2,5-dihydroxybenzenesulfonate). The active pharmaceutical ingredient (API) is introduced to the base formulation via spatulation.
Formulations D-F: Propylene glycol, transcutol and a combinat...
example 2
In Vitro Percutaneous Absorption of Potassium 2,5-Dihydroxybenzenesulfonate from Various Formulations
[0174]Formulations were tested that differ in the approach used for physically stabilizing Formulation 2567-95 (shown in Table 4 below). The in vitro percutaneous absorption of 2,5-dihydroxybenzenesulfonate was characterized from eight formulations at 10% potassium 2,5-dihydroxybenzenesulfonate and one reference formulation (Formulation 2567-95, 5% potassium 2,5-dihydroxybenzenesulfonate) following topical application to excised human skin from elective surgery.
Methods
[0175]This in vitro percutaneous absorption study evaluated tissue permeation and penetration of 2,5-dihydroxybenzenesulfonate from various formulations. The composition of each of the formulations evaluated in this study is summarized in Table 4.
TABLE 4Formulation Compositions123456789Lot # 2567-958689879190929394IngredientsControlIn SolutionSuspendedPotassium Dobesilate51010101010101010Cetyl Alcohol2.50.50.50.50.50.50...
example 3
Formulation Preparation Methods
[0184]A formulation of the invention may be prepared using the non-limiting methods disclosed below, which are intended to illustrate certain embodiments of the invention.
[0185]Preparation of formulation # 2567-87, a solution, discussed above may be carried out as follows.
Formulation #2567-87
[0186]
Ingredients% w / wA.DI Water31.4100 mM Acetate10.0Buffer (pH 4.0)Sodium Thiosulfate,0.1PenatahydrateB.Potassium 2,5-10.0dihydroxybenzenesulfonateC.Benzyl Alcohol0.5D.Cetyl Alcohol0.5Stearyl Alcohol2.5White Petrolatum20.0Mineral Oil20.0Brij 721.0Brij 7214.0
[0187]Procedure:
[0188]1. Combine ingredients in phase A in an appropriate size beaker and propeller mix until a solution is achieved (approximately 30 minutes).
[0189]2. In a laminar flow hood, add API in phase B to step 1. Once API is properly wetted, remove from hood and propeller mix until solution is achieved (approximately a few hours). Add heat (water bath) if necessary to speed up disillusion process. He...
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