Unlock instant, AI-driven research and patent intelligence for your innovation.

High-density melamine foam and preparation method thereof

a melamine foam, high-density technology, applied in the a preparing method, can solve the problems of limiting the application field of melamine foam, density and strength are still difficult to adapt to the higher requirements, and achieve the effects of increasing the molecular weight and functionality of resin, increasing solid content, and improving the density and strength of melamine foam

Inactive Publication Date: 2016-11-10
CHENGDU YULONG CHEM
View PDF1 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The present invention concerns a method for making melamine foam using a specific mixture of raw materials that increases its thickness, solid content, and functionality. This results in a stronger and more dense foam that is useful in a variety of applications such as thermal insulation, sound insulation, and decoration. It can also be used in industrial settings for heat and cold insulation, and in civil settings for cleaning and sanitation. Additionally, it is suitable for use in cushions and sofas.

Problems solved by technology

In practical applications, some fields, such as cushion, sofa, thermal insulation, cleaning and other fields, make higher requirements for the density and strength of melamine foam, but the density of the melamine foam on the current market is generally 4 to 10 kg / m3, which is difficult to meet the requirements, thereby limiting the application fields of the melamine foam.
The above-mentioned patent technology proposes the preparing method of melamine foam, but the density and strength are still difficult to adapt to the higher requirements.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

embodiment 1

[0023]The high-density melamine foam is prepared according to the following steps:[0024](1) Preparing 3200 g of primary polymer of waterborne melamine formaldehyde resin according to a conventional method, wherein the solid content of the waterborne melamine formaldehyde resin is 75%, and the molar ratio of formaldehyde to melamine in raw materials for preparing the waterborne melamine formaldehyde resin is 3:1;[0025](2) Uniformly mixing the primary polymer of the waterborne melamine formaldehyde resin with 80 g of alkylphenol ethoxylates (OP-10 for short) and 8 g of dicyandiamide in a thermostatic mixing tank to obtain a mixture A, wherein the stirring rotating speed 250 r / min, and the temperature of the mixture A is 30° C.;[0026](3) Transferring the mixture A and 800 g of tetramethylol melamine to a thermostatic twin-screw extruder through a metering transfer pump and a metering feeder respectively to uniformly mix to obtain a mixture B, wherein the mixing rotating speed is 150 r / ...

embodiment 2

[0031]The high-density melamine foam is prepared according to the following steps:[0032](1) Preparing 2000 g of primary polymer of waterborne melamine formaldehyde resin according to a conventional method, wherein the solid content of the waterborne melamine formaldehyde resin is 78%, and the molar ratio of formaldehyde to melamine in raw materials for preparing the waterborne melamine formaldehyde resin is 3:1;[0033](2) Uniformly mixing the primary polymer of the waterborne melamine formaldehyde resin with 188 g of desalted water, 120 g of sodium lauryl polyoxyethylene ether sulfate (AES for short) and 20 g of talcum powder in a thermostatic mixing tank to obtain a mixture A, wherein the stirring rotating speed is 250 r / min, and the temperature of the mixture A is 30° C.;[0034](3) Transferring the mixture A and 2000 g of tetramethylol melamine to a thermostatic twin-screw extruder through a metering transfer pump and a metering feeder respectively to uniformly mix to obtain a mixtu...

embodiment 3

[0038]The high-density melamine foam is prepared according to the following steps:[0039](1) Preparing 2000 g of primary polymer of waterborne melamine formaldehyde resin according to a conventional method, wherein the solid content of the waterborne melamine formaldehyde resin is 73%, and the molar ratio of formaldehyde to melamine in raw materials for preparing the waterborne melamine formaldehyde resin is 2:1;[0040](2) Uniformly mixing the primary polymer of the waterborne melamine formaldehyde resin with 68 g of ethyl alcohol, 80 g of sodium dodecyl sulfate, 40 g of dodecyl polyethenoxy ether, 8 g of dicyandiamide and 20 g of talcum powder in a thermostatic mixing tank to obtain a mixture A, wherein the stirring rotating speed is 250 r / min, and the temperature of the mixture A is 33° C.;[0041](3) Transferring the mixture A with 1000 g of tetramethylol melamine and 1000 g of hexamethylol melamine which are pre-mixed to a thermostatic twin-screw extruder through a metering transfer...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
boiling pointaaaaaaaaaa
temperatureaaaaaaaaaa
temperatureaaaaaaaaaa
Login to View More

Abstract

The present invention discloses high-density melamine foam, which comprises the following raw materials; a primary polymer of waterborne melamine formaldehyde resin, solid methylol melamine, a polar solvent, a surfactant, a foaming agent, a curing agent and an additive. The present invention also discloses a preparing method of the high-density melamine foam, comprising the following steps: preparing a primary polymer of waterborne melamine formaldehyde resin; uniformly mixing the primary polymer of the waterborne melamine formaldehyde resin, the polar solvent, the surfactant and the additive to obtain a mixture A; uniformly mixing the mixture A with the solid methylol melamine to obtain a mixture B; uniformly mixing the mixture B with the foaming agent to obtain a mixture C; uniformly mixing the mixture C with the curing agent to obtain a mixture D; and carrying out microwave radiation, foaming, curing, drying and quenching on the mixture D in a microwave foaming device to obtain the high-density melamine foam. The melamine foam described in the present invention has high density and high strength performance.

Description

CROSS-REFERENCE TO RELATED APPLICATIONS[0001]This application is a continuation of, and claims priority to, Chinese Patent Application No. 201510228178.6 with a filing date of May 7, 2015. The content of the aforementioned application, including any intervening amendments thereto, is incorporated herein by reference.TECHNICAL FIELD[0002]The present invention relates to melamine foam and a preparing method thereof, and particularly to high-density melamine foam and a preparing method thereof.BACKGROUND[0003]The existing melamine foam is low-density and high-open-ratio flame-retardant foam, has excellent flame retardant, sound absorption, thermal insulation and cleaning functions, and can be widely applied to the construction, transportation, household and industry fields. In practical applications, some fields, such as cushion, sofa, thermal insulation, cleaning and other fields, make higher requirements for the density and strength of melamine foam, but the density of the melamine f...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(United States)
IPC IPC(8): C08J9/00C08J3/28C08J3/20
CPCC08J9/0014C08J2361/28C08J3/28C08J3/203B29C44/3442C08J9/04C08J2201/03
Inventor YE, RUIZHANG, LUGOU, HANGSU, HUAFU, HAO
Owner CHENGDU YULONG CHEM