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43 results about "Carbon isotope composition" patented technology

Method and apparatus for performing rapid isotopic analysis via laser spectroscopy

Method and apparatus for providing real-time data indicative of the isotopic composition of formation fluids during drilling. The method includes the steps of: (a) providing a reference fluid having a known isotopic composition in a reference cell; (b) capturing a sample of formation; (c) providing at least one laser beam; (e) passing a beam through the reference fluid, measuring the reference-measurement beam before and after it passes through the reference fluid; (f) and passing a beam through the sample, measuring the beam before and after it passes through the sample, and calculating a first isotope concentration from those measurements. The measurements can provide information relating to the carbon isotopic composition of individual compounds in hydrocarbon gas mixtures, with the individual compounds including methane, ethane, propane, iso- or normal butane, or iso- or normal pentane.
Owner:CALEB BRETT USA

Method by utilizing double markers to acquire share of inorganic carbon source utilized by plants

The invention discloses a method by utilizing double markers to acquire share of inorganic carbon source utilized by plants, which comprises the following steps that: A. sodium bicarbonate produced by different manufacturers is determined, two types of sodium bicarbonate with delta 13C difference being more than eight thousandths are used as an isotopic marker 1 and an isotopic marker 2 to be respectively added into nutrient fluid to culture plants; delta 13C value of bicarbonate ion in nutrient fluid of the isotopic marker 1 is delta C1, and delta 13C value of bicarbonate ion in nutrient fluid of the isotopic marker 2 is delta C2; and B. after more than four leaves appear, the values of delta 13C consisting of stable carbon isotopes of plant leaves to be observed correspondently culturedby the nutrient fluid of the two types of isotopic markers are respectively determined as delta T1 and delta T2; and C. delta C1, delta C2, delta T1 and delta T2 are brought into equation fB= to calculate the share fB of the carbonate ions utilized by the plants. Due to the adoption of the method, the share of the inorganic carbon source utilized by the plants can be rapidly acquired, the steps are fewer, simplicity in calculation can be realized, and data is reliable.
Owner:INST OF GEOCHEM CHINESE ACADEMY OF SCI

Method for measuring bicarbonate ion utilizing capability of plant

InactiveCN101926267ALittle plant materialSmall footprintHorticulture methodsMaterial analysisProportional shareIsotope
The invention discloses a method for measuring the bicarbonate ion utilizing capability of a plant. The method comprises the following steps of: (1) respectively measuring stable carbon isotope compositions, i.e. delta 13C values of leaves of a plant to be studied and a reference plant; (2) measuring the stable carbon isotope composition, i.e. delta 13C value of microalgae; (3) substituting the delta 13C value of the leaves of the plant to be studied, the delta 13C value of the leaves of the reference plant and the delta 13C value of the microalgae into a two-end-member model and calculating the proportional share of bicarbonate ions utilized by the plant to be studied in an inorganic carbon source; (4) measuring the net photosynthetic rate of the leaves of the plant to be studied; and (5) deriving the bicarbonate ion utilizing capability of the plant to be studied according to the net photosynthetic rate of the leaves of the plant to be studied and the proportional share of the bicarbonate ions utilized by the plant to be studied in the inorganic carbon source. The invention can be used for quantitatively measuring the bicarbonate ion utilizing capability of the plant with less plant materials and less steps and simple calculation.
Owner:INST OF GEOCHEM CHINESE ACADEMY OF SCI

Method for analyzing source of secondary organic carbon in ambient air fine particles

InactiveCN103226128AAvoid errorsThe analysis results are accurate and reliableMaterial analysis by electric/magnetic meansSoil scienceFine particulate
The invention relates to a method for analyzing a source of secondary organic carbon in ambient air fine particles. The method comprises: determining concentrations and stable carbon isotope compositions of organic carbon and elemental carbon in ambient air fine particle PM2.5; calculating to obtain stable carbon isotope composition of secondary organic carbon in the ambient air fine particle PM2.5; and finally adopting a stable carbon isotope technology to analyze a source of the secondary organic carbon in the ambient air fine particle PM2.5. According to the present invention, a binary composite isotope mass balance model is adopted to calculate the carbon isotope composition of the secondary organic carbon, such that problems that the secondary organic carbon is difficultly separated from the organic carbon and determination of the carbon isotope composition of the secondary organic carbon is difficult are solved, a new method for analyzing the source of the secondary organic carbon is provided, and problems that tracers are limited and identification is difficult of the existing organic molecule tracer method are avoided.
Owner:TAIYUAN UNIV OF TECH

Carbon isotope analysis method for series of hydrocarbon compounds in natural gas

InactiveCN103913534AEfficient analysisFast and effective methodComponent separationIsotopeQualitative analysis
The invention belongs to the technical field of analysis methods for natural gas and especially relates to a carbon isotope analysis method for a series of hydrocarbon compounds in natural gas. The method comprises the following steps: step A, carrying out solid-phase micro-extraction enrichment on a series of hydrocarbon compounds in natural gas; step B, separating the hydrocarbon compounds and carrying out qualitative analysis on unknown hydrocarbon compounds; and step C, carrying out carbon isotope determination on the hydrocarbon compounds. According to the invention, solid-phase micro-extraction technology is introduced into a natural gas isotope analysis method and combined with a GC-IRMS analysis system, influence of factors like equilibrium time and equilibrium temperature on difference of adsorption capability of the hydrocarbon compounds and on carbon isotope values are analyzed, and operation conditions are optimized, so effective enrichment and carbon isotope composition analysis of the series of hydrocarbon compounds in natural gas are realized. The method provided by the invention can realize rapid and effective enrichment and carbon isotope composition analysis of the series of hydrocarbon compounds in natural gas.
Owner:LANZHOU CENT FOR OIL & GAS RESOURCES INST OF GEOLOGY & GEOPHYSICS CAS

Oil source comparison method

The invention discloses an oil source comparison method and belongs to the technical field of exploration. The invention solves a technical problem of low accuracy of a comparison result of oil sources in the prior art. The oil source comparison method comprises the steps of: 1) performing group component separation of crude oil and potential source rocks, and measuring the quantities of stable carbon isotopes of all the separated group components; 2) calculating the composition of stable carbon isotopes of all group components in the crude oil and the potential source rocks; 3) by means of the composition of stable carbon isotopes in the same group component in the crude oil and the potential source rocks, calculating relationship coefficient of the same group component in the crude oil and the potential source rocks; and 4) according to the relationship coefficient of stable carbon isotope composition the same group component in the crude oil and the potential source rocks, determining the relationship of the crude oil and the potential source rocks.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for detecting and quantifying utilization of carbon source in calcium carbonate by microalgae

The invention discloses a method for detecting and quantifying utilization of carbon source in calcium carbonate by microalgae. The method comprises the following steps: adding two types of calcium carbonate powder with great difference in Epsilon 13 C value but same crystal form respectively to cultivate the to-be-detected microalgae, measuring the protein content of the microalage at different incubation time and Epsilon 13 C value of the stable carbon isotope composition of the microalage after a harvest; then, remedying the measured Epsilon 13 C value of the microalage at the time of the harvest by using the protein content of the initial microalage and Epsilon 13 C value, and obtaining the share of carbon source in the added calcium carbonate utilized by the microalgae by using the isotope mixed model; through the data about the protein content of the microalage at different incubation time and Redfield value, fitting an exponential growth equation about the biomass and time; finally, calculating the amount of carbon source in calcium carbonate obtained by the detected microalgae of biomass per unit in unit time according to the share of carbon source in the added calcium carbonate utilized by the microalgae and the equation about the biomass and time.
Owner:INST OF GEOCHEM CHINESE ACADEMY OF SCI

Determination method for fractional value of stable carbon isotopes in carbon dioxide assimilation process of microalgae

The invention discloses a determination method for the fractional value of stable carbon isotopes in the carbon dioxide assimilation process of microalgae. The determination method comprises the following steps: respectively adding two types of sodium bicarbonate with large delta<13>C value difference into a detection culture solution added with 10mM acetazolamide to culture the microalgae to be detected; obtaining a composition of the stable carbon isotopes of a newly born algae body of detected microalgae cultured in the detection culture solution labelled by two types of isotopes and the portion of added inorganic carbon source utilized by the microalgae to be detected; according to the result and the composition of the average stable carbon isotopes of atmospheric carbon dioxide in the culture environment during the culture period, obtaining the fractional value of the stable carbon isotopes in the carbon dioxide assimilation process of the microalgae. The determination method disclosed by the invention has the advantages that the fractional value of the stable carbon isotopes can be determined in vivo, and not only can the fractional value of the stable carbon isotopes of a single microalgae seed be detected, but also the fractional value of the stable carbon isotopes of mixed microalgaes can be detected, and the detected data are reliable and the accuracy of a result is high.
Owner:INST OF GEOCHEM CHINESE ACADEMY OF SCI

Method for identifying stable carbon isotope composition of isoprene in atmosphere

The invention discloses a method for determining stable carbon isotope composition of isoprene in atmosphere, comprising the following steps: step I: determining the stable carbon isotope composition of 2-methyl butantetraol in aerosol; step B: determining an isotopic fractionation constant of 2-methyl butantetraol generated by isoprene through photochemical reaction; and step C: calculating the stable carbon isotope composition of the isoprene in the atmosphere. The method can be used for analyzing a source of the isoprene in the atmosphere, discussing a migration and transfer rule, and researching and exploring distribution of vegetations (C3, C4 and CAM) with different photosynthesis types in an environment. The method solves the difficult problem that the stable carbon isotope composition of the active volatile organic compound in the atmosphere is hard to determine accurately and establishes a method foundation for explaining generation, migration, transfer and trend rules of the isoprene in nature.
Owner:SICHUAN AGRI UNIV

Method for measuring daily mean stable carbon isotope composition of atmospheric carbon dioxide

The invention discloses a method for measuring the daily mean stable carbon isotope composition of atmospheric carbon dioxide, which is characterized by comprising the steps of (I) measuring sodium bicarbonate produced by different manufacturers as tracer agents; (II) adding sodium bicarbonate into a nutrient solution respectively, and setting the concentration of sodium bicarbonate in the nutrient solution to 10mM and the pH value to 8.30; (III) cultivating the plants with same growth cycle by use of the prepared solution at the same time, and after 24 hours of cultivation, separately measuring the values of the stable carbon isotope composition (delta)13C in two isotope-labeled nutrition solutions, namely a value of (delta)1 and a value of (delta)2; (IV) substituting the measured values of (delta)C1, (delta)C2, (delta)1 and (delta)2 into an equation, and calculating the proportion fB of added sodium bicarbonate to total inorganic carbon in the solution; (V) judging whether the value of fB is less than 0.6, fetching the measured values obtained by an experiment when the value of fB is less than 0.60, substituting the measured values into an equation, and calculating the average value of inorganic carbon (delta)13C entering the culture solution in atmospheric carbon dioxide within the time period (delta)a; (VI) substituting the calculated (delta)a into an equation (delta)Ca=(delta)a+(Delta)CO2(air)-HCO3(aq), and calculating the daily mean stable carbon isotope composition (delta)Ca of atmospheric carbon dioxide.
Owner:INST OF GEOCHEM CHINESE ACADEMY OF SCI

Detection method for isotopes of exogenous benzoic acid in dairy product

ActiveCN105486825AAids in source detectionSimplify the judgment procedureTesting dairy productsBenzoic acidFractionation
The invention relates to a detection method for isotopes of exogenous benzoic acid in a dairy product. Specifically, the detection method is a technology for detecting adulteration and doping of food based on a stable isotope technology. The method is established on the basis of the theory of natural fractionation characteristics and metabolism process of stable carbon isotopes. A relation model for carbon isotope composition of benzoic acid and casein naturally existing in the dairy product method is constructed by determining stable carbon isotope composition of major constituents and benzoic acid in the dairy product, and determination is carried out based on the relation between delta<13> values of benzoic acid and casein in a sample. The detection method is accurate and reliable and can be used for rapid detection of exogenous added benzoic acid in the dairy product.
Owner:CHINA NAT RES INST OF FOOD & FERMENTATION IND CO LTD

Method for detecting exogenously added ethyl caproate and ethyl lactate in liquor

The invention relates to a method for detecting exogenously added ethyl caproate and ethyl lactate in liquor on the basis of a stable isotope technique and principle and belongs to the technical field of authenticity identification of liquor. The method mainly comprises steps as follows: (1), the carbon isotope composition of a target chemical compound (ethyl caproate and / or ethyl lactate) in a fragrance type real liquor sample is detected, and the carbon isotope composition of a carbon isotope endogenous marker of the target chemical compound is detected, and the average difference of delta13C values between the target chemical compound and an internal standard substance as well as the standard deviation sigma is determined; (2), delta13C values of the target chemical compound and the internal standard substance of the target chemical compound in the to-be-detected liquor sample are detected, and the difference value delta13C (to-be-detected sample) of the target chemical compound and the internal standard substance is calculated; (3), whether the to-be-detected sample contains the exogenously added ethyl caproate and / or ethyl lactate is judged. The method used for effectively detecting whether the liquor contains exogenously added ethyl caproate and / or ethyl lactate is established with a stable isotope technique.
Owner:CHINA NAT RES INST OF FOOD & FERMENTATION IND CO LTD

Method for detecting exogenously-added ethyl caproate in baijiu

The invention relates to a method for detecting exogenously-added ethyl caproate in baijiu on the basis of the stable isotope technology and principle, and belongs to the technical field of baijiu authenticity identification. The method mainly comprises the following steps that 1, the carbon isotope composition of a target compound (ethyl caproate) in a real baijiu sample of one certain odor type is detected, the carbon isotope composition of a carbon isotope endogenous marker of the target compound is detected, and the average difference and standard deviation (sigma) of delta 13 C values of the target compound and the internal standard substance are determined; 2, the delta 13 C values of a target compound and an internal standard substance in a baijiu sample to be detected are detected, and the difference value delta 13 C of the sample to be detected is calculated; 3, whether the sample to be detected contains exogenously-added ethyl caproate or not is judged. By means of the stable isotope technology, the method capable of accurately detecting whether baijiu contains exogenously-added ethyl caproate or not is built.
Owner:CHINA NAT RES INST OF FOOD & FERMENTATION IND CO LTD

Laser Raman detection method for quantitative analysis of CO2 gas carbon isotope composition

The invention provides a laser Raman detection method for quantitative analysis of a CO2 gas carbon isotope composition, comprising the following steps: 1, calculating Raman quantification factor F12CO2 of 12CO2; 2, calculating Raman quantification factor F13CO2 of 13CO2; 3, calculating the mole ratio C[12CO2] / C[13CO2] of 12CO2 and 13CO2 in CO2 gas according to the formulation of C[12CO2] / C[13CO2]=(Al2CO2 / Al3CO2)*(F13CO2 / F12CO2). The detection method disclosed by the invention is used for microscopic laser Raman test analysis on 12CO2 / N2 mixed gas and 13CO2 / N2 mixed gas in different proportions, the adopted microscopic laser Raman spectroscopy has the characteristics of high precision, in-situ detection, no loss, rapidness and the like, and the CO2 gas carbon isotope composition can be quantitatively analyzed by utilizing the microscopic laser Raman spectroscopy. The laser Raman detection method disclosed by the invention has a wide application prospect.
Owner:CHANGAN UNIV

Carbon isotope method for tracing aldehyde ketone pollutants

The invention discloses a carbon isotope method for tracing aldehyde ketone pollutants. The method is characterized in that sources of aldehyde ketone pollutants in atmosphere environment are judged according to occurrence of isotope fractionation or not and the difference of the carbon isotope ratio (delta<13>C value). An experiment result shows that the method has the advantages of good recurrence and high precision of a determination result, and effective overcoming of the defects of traditional concentration measurement methods (EPA TO-11A), can be used to determine the carbon isotope composition (delta<13>C value) of atmosphere aldehyde ketone pollutants in order to realize direct and accurate judgment of the sources of the atmosphere aldehyde ketone pollutants, can be used to trace the sources of the atmosphere aldehyde ketone pollutants as an effective way, is helpful for researching the formation mechanism of atmosphere organic pollution, and provides scientific bases for researches of the atmosphere organic environment pollution.
Owner:GUANGXI UNIV

Carbon nanotube array and method for making same

A carbon nanotube array is provided. The carbon nanotube array includes at least two isotope-doped carbon nanotube sub-arrays. Each isotope-doped carbon nanotube sub-array includes a plurality of carbon nanotubes. The carbon nanotubes in different isotope-doped carbon nanotube sub-array are composed of different kinds of carbon isotopes. The present disclosure also provides a method for making the carbon nanotube arrays.
Owner:TSINGHUA UNIV +1

Determination device and determination method for carbon dioxide carbon isotope composition in mineral inclusion

The invention belongs to the technical field of determination of carbon dioxide and carbon isotope composition in mineral inclusion, and particularly relates to a determination device and a determination method for carbon dioxide and carbon isotope composition in mineral inclusion. The device comprises a first helium inlet, a first valve, a first water trap, a second helium inlet, a second valve, a second water trap, a third water trap, a temperature control heating furnace, a six-way valve, a carbon dioxide trap, a single-opening quartz tube, a carbon dioxide collecting tube, a liquid nitrogen cup, a stable isotope mass spectrometer, a sample injection needle, a sample tube and a plurality of connecting pipelines. A continuous flow sampling device is adopted, a mineral inclusion bursting device and the carbon dioxide collecting device are connected with the stable isotope mass spectrometer, and online heating bursting of the mineral inclusion, online collecting of carbon dioxide gas and online testing of carbon dioxide carbon isotope are achieved.
Owner:BEIJING RES INST OF URANIUM GEOLOGY

Online continuous flow analysis and extraction device and method for methane carbon isotope composition in gas

The invention belongs to the technical field of determination of carbon isotope composition of methane in gas, and particularly discloses an online continuous flow extraction device for methane in gasand a carbon isotope composition analysis method. The device comprises a first six-way valve, a plurality of helium inlets communicated with the first six-way valve, a second six-way valve communicated with the first six-way valve, a helium inlet communicated with the second six-way valve, a carbon dioxide collecting pipe communicated with the second six-way valve, a single-opening quartz tube communicated with the second six-way valve, and a stable isotope mass spectrometer communicated with the second six-way valve. The method comprises the following steps of: 1, loading a gas sample; 2, conducting blow-back degassing, and completely exhausting air in pipelines at the two ends of a gas collecting pipe; 3, oxidizing, purifying and collecting methane in the gas; 4, sublimating and injecting carbon dioxide; and 5, determining methane carbon isotopes. According to the invention, the problems of excessive use amount of off-line pretreatment sample preparation gas, complicated operation process and low efficiency are solved.
Owner:BEIJING RES INST OF URANIUM GEOLOGY

Method for detecting exogenously-added ethyl lactate in baijiu

The invention relates to a method for detecting exogenously-added ethyl lactate in baijiu on the basis of the stable isotope technology and principle, and belongs to the technical field of baijiu authenticity identification. The method mainly comprises the following steps that 1, the carbon isotope composition of a target compound (ethyl lactate) in a real baijiu sample of one certain odor type is detected, the carbon isotope composition of a carbon isotope endogenous marker of the target compound is detected, and the average difference and standard deviation (sigma) of delta 13 C values of the target compound and the internal standard substance are determined; 2, the delta 13 C values of a target compound and an internal standard substance in a baijiu sample to be detected are detected, and the difference value delta 13 C of the sample to be detected is calculated; 3, whether the sample to be detected contains exogenously-added ethyl lactate or not is judged. By means of the stable isotope technology, the method capable of accurately detecting whether baijiu contains exogenously-added ethyl lactate or not is built.
Owner:CHINA NAT RES INST OF FOOD & FERMENTATION IND CO LTD

Aromatic hydrocarbon purification method suitable for analyzing specific carbon isotope

The invention relates to an aromatic hydrocarbon purification method suitable for analyzing a specific carbon isotope. The method comprises the following steps: (1) adding crude oil into a clean glass tube, removing air in the glass tube by virtue of helium replacement, vacuumizing, and sealing; (2) heating the glass tube filled with the crude oil in step (1) in a muffle furnace to obtain pyrolysis products; (3) cooling the pyrolysis products to a room temperature, ultrasonically extracting for 2 to 4 times by using dichloromethane, and merging to obtain extract liquid; and (4) concentrating the extract liquid, precipitating asphaltene by using n-hexane after the concentration of the extract liquid, directly analyzing components of the aromatic hydrocarbon (GC-MS) and testing the specific carbon isotope (GC-IRMS). The aromatic hydrocarbon purification method is low in cost, easy to implement, wide in application range, and capable of providing an effective technical means for the comparison of an oil source consisting of substituent-free aromatic hydrocarbon specific carbon isotopes in a deep oil-gas zone.
Owner:LANZHOU CENT FOR OIL & GAS RESOURCES INST OF GEOLOGY & GEOPHYSICS CAS

Shale gas dessert evaluation method based on gaseous carbon isotope

ActiveCN111622751ALower Exploration CostsShorten dessert evaluation cycleSurveyConstructionsPhysical chemistryShale gas
The invention discloses a shale gas dessert evaluation method based on gaseous carbon isotope. The method comprises the steps that gaseous carbon isotope composition data are obtained in a while-drilling manner; geologic logging data are collected; the gaseous carbon isotope composition data and the geologic logging data draw a composite profile; and in combination with geological parameters, according to gaseous carbon isotope composition parameters, the dessert interval is divided. Through the above manner, the method can be implemented after a straight well is completed, the dessert evaluation period can be effectively shortened, and the oil and gas exploration efficiency is improved.
Owner:苏州冠德能源科技有限公司

A method for obtaining the utilization share of plant bicarbonate in wild habitat

The invention discloses a method for acquiring bicarbonate using share of plants in field habitat, and belongs to the field of crop information detection technologies and ecological environmental management. The method includes acquiring extracellular atmospheric carbon dioxide concentration and intercellular carbon dioxide concentration data by the aid of portable photosynthetic apparatuses, measuring air carbon dioxide and soil bicarbonate using stable carbon isotope fractionation values of the plants at different seedling ages and different growth periods in different environments, and combining atmospheric carbon dioxide stable carbon isotope composition and rhizosphere soil bicarbonate stable carbon isotope composition of the plants with each other; acquiring instant information of the bicarbonate using share of the plants at the different seedling ages and the different growth periods in the different environments according to double-end-member isotope hybrid models. The method has the advantages that atmospheric carbon dioxide using share of the plants at the different seedling ages and the different growth periods in the field habitat can be quickly, conveniently and accurately acquired in real time by the aid of the method, and the bicarbonate using share of the plants in the field habitat also can be acquired by the aid of the method.
Owner:INST OF GEOCHEM CHINESE ACADEMY OF SCI

Method and system for high-resolution determination of organic carbon isotopes in stalagmite

The invention discloses a method and a system for high-resolution determination of organic carbon isotopes in stalagmite. The method comprises the following steps: loading a stalagmite powder sample into an inverted Y-shaped sample bottle; at the bottom of a first branch, adding 1 mol / L of hydrochloric acid into the stalagmite powder sample; after chromic acid is added to the bottom of a second branch, screwing a bottle pad and a bottle cap which are used for sealing to the first branch; connecting the first branch with a vacuum pipeline of a vacuum system; separating the vacuum system from the first branch, and then inserting a double-hole needle into the bottle cap and the bottle pad; filling the sample bottle with helium through the double-hole needle; fully mixing chromic acid in the second branch with the acidified stalagmite powder sample in the first branch; and inserting the double-hole needle into the bottle cap and the bottle pad. Organic CO2 flowing through a silver wire purification tube is enriched and purified, and then is introduced into a mass spectrometer to determine the carbon isotope composition, so that high-resolution determination of the organic carbon isotope in the stalagmite powder sample is realized.
Owner:INST OF GEOLOGY & GEOPHYSICS CHINESE ACAD OF SCI

A method for analyzing carbon isotopes of series hydrocarbons in natural gas

The invention belongs to the technical field of analysis methods for natural gas and especially relates to a carbon isotope analysis method for a series of hydrocarbon compounds in natural gas. The method comprises the following steps: step A, carrying out solid-phase micro-extraction enrichment on a series of hydrocarbon compounds in natural gas; step B, separating the hydrocarbon compounds and carrying out qualitative analysis on unknown hydrocarbon compounds; and step C, carrying out carbon isotope determination on the hydrocarbon compounds. According to the invention, solid-phase micro-extraction technology is introduced into a natural gas isotope analysis method and combined with a GC-IRMS analysis system, influence of factors like equilibrium time and equilibrium temperature on difference of adsorption capability of the hydrocarbon compounds and on carbon isotope values are analyzed, and operation conditions are optimized, so effective enrichment and carbon isotope composition analysis of the series of hydrocarbon compounds in natural gas are realized. The method provided by the invention can realize rapid and effective enrichment and carbon isotope composition analysis of the series of hydrocarbon compounds in natural gas.
Owner:LANZHOU CENT FOR OIL & GAS RESOURCES INST OF GEOLOGY & GEOPHYSICS CAS

A method for detecting exogenously added ethyl lactate in liquor

The invention relates to a method for detecting exogenously added ethyl caproate and ethyl lactate in liquor on the basis of a stable isotope technique and principle and belongs to the technical field of authenticity identification of liquor. The method mainly comprises steps as follows: (1), the carbon isotope composition of a target chemical compound (ethyl caproate and / or ethyl lactate) in a fragrance type real liquor sample is detected, and the carbon isotope composition of a carbon isotope endogenous marker of the target chemical compound is detected, and the average difference of delta13C values between the target chemical compound and an internal standard substance as well as the standard deviation sigma is determined; (2), delta13C values of the target chemical compound and the internal standard substance of the target chemical compound in the to-be-detected liquor sample are detected, and the difference value delta13C (to-be-detected sample) of the target chemical compound and the internal standard substance is calculated; (3), whether the to-be-detected sample contains the exogenously added ethyl caproate and / or ethyl lactate is judged. The method used for effectively detecting whether the liquor contains exogenously added ethyl caproate and / or ethyl lactate is established with a stable isotope technique.
Owner:CHINA NAT RES INST OF FOOD & FERMENTATION IND CO LTD
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