Pulp using rice grass and wheatgrass as raw material and preparation method thereof
A pulp and wheat straw technology, which is applied in the fields of cellulose raw material pulping, textile and paper making, and fiber raw material processing, etc., can solve the problems of lack of involvement.
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Embodiment 1
[0044] After the dry preparation, the rice straw is mixed and impregnated with the ammonium sulfite solution of 9% absolute dry rice straw in the dipping screw machine through the dipping screw machine, and then sent to the steaming ball. 0.6%, the liquid ratio is 1:3, the steaming ball is idling for 20 minutes after the straw is filled; after that, the steam is heated once to raise the temperature to 100°C, and the temperature is kept at this temperature for 30 minutes, and then the steam is released for 20-30 minutes. Start steaming for the second heating, raise the temperature for 30 minutes to 165°C, and keep warm for 80 minutes; add black liquor to the steaming ball to adjust the concentration, adjust the concentration to 10%, and keep the pressure at 0.75MPa for spraying, at this time The hardness of the pulp is potassium permanganate value 20, which is equivalent to a kappa value of 32, the pH value at the end of cooking is 11, the residual alkali concentration in the bl...
Embodiment 2
[0046] The wheat straw after preparing materials by the method is sent into the steaming ball, and the caustic soda solution of 10% to the absolute dry raw material is added in the steaming ball, the addition of anthraquinone is 0.7% of the absolute dry raw material, the liquid ratio is 1:4, and the wheat straw is filled Afterwards, the steaming ball is idling for 20 minutes; after that, heat up to 110°C with steam, keep warm at this temperature for 20 minutes, and let off steam for 20-30 minutes, start steaming for the second heating, and raise the temperature for 30 minutes to reach the temperature at 168°C, keep warm for 90 minutes; add black liquor into the steaming ball to dilute, and at the same time keep the pressure at 0.75MPa for spraying. The pH value is 12 and the residual alkali concentration in the black liquor is 12 g / l. The yield of the prepared high hardness pulp was 62%. The wheat straw is cooked by the ammonium method, and the hardness of the wheat straw pul...
Embodiment 3
[0048] After the dry preparation, the straw is mixed and impregnated with a mixture of 12% sodium hydroxide solution and black liquor in the dipping auger. The waste liquid extracted from the straw is then sent to the steaming ball, the amount of anthraquinone added is 0.8% of the absolute dry raw material, the liquid ratio is 1:2.5, and the steaming ball is idling for 20 minutes after the straw is filled; after that, the steam is heated once , heat up to 120°C, keep warm at this temperature for 40 minutes, then let off steam for 20-30 minutes, start to pass steam for the second heating, raise the temperature for 30 minutes to 173°C, keep warm for 90 minutes; keep the pressure at 0.75MPa for spraying . Now the hardness of pulp is potassium permanganate value 17 which is equivalent to kappa number 25, meanwhile, the pH value is 12 when cooking end point, and the residual alkali concentration in the black liquor is 14g / l. The yield of the high hardness pulp is 64%. Then add bl...
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