Chlorine resistant polyurethaneurea composition
A polyurethane urea and elastic fiber technology, applied in the direction of single-component polyurethane rayon, single-component synthetic polymer rayon, spinning solution preparation, etc., can solve the problem of increased filtration pressure and fiber breakage rate, poor dispersion, and product Yellowing and other problems, to achieve the effect of inhibiting fiber coloring or decolorization, preventing moisture absorption, and reducing secondary aggregation
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Embodiment 1
[0066] Polytetramethylene ether glycol (PTMEG, molecular weight 1815) and diphenylmethane-4,4'-diisocyanate (MDI) were added and polymerized at a molar ratio of 1.70 (NCO / OH=1.70) to prepare terminal untreated The reacted diisocyanate does not exceed 3.0 mole percent of the primary polymer. The primary polymer was homogeneously dissolved in N,N-dimethylacetamide (DMAc) in a high-performance dissolver to obtain a primary polymer mixture in which the content of unreacted diisocyanate had been constantly adjusted to 2.64 ± 0.02 mol%. Ethylenediamine and 1,2-diaminopropane as chain extenders and diethylamine as chain terminator were dissolved in DMAc, and this mixture was fed to the secondary polymerizer along with the primary polymer mixture. Through the conventional polymerization process of polyurethane urea elastic fiber, the solid content of the polymer is about 35wt%, and the apparent viscosity at 40°C is about 2000-3500 poise. The intrinsic viscosity measured in N,N-dimet...
Embodiment 2
[0071] Elastic fibers were prepared according to the same method as described in Example 1, except that hydromagnesite (Airlite-S3, obtained from Nanotech Ceramics) with an average particle size of not more than 10 μm coated with stearic acid by a wet method was used As a chlorine resistant material.
Embodiment 3
[0073] Elastic fibers were prepared according to the same method described in Example 1, except that uncoated hydromagnesite (Airlite-S3, available from Nanotech Ceramics) with an average particle size of not more than 10 μm was used as the chlorine-resistant material.
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