Method for separating and purifying nonane diacid
A technology for separation and purification of azelaic acid, which is applied in the separation/purification of carboxylic acid compounds, organic chemistry, and preparation of carboxylic acids by ozone oxidation. It can solve the problems of azelaic acid loss and other problems, and achieve short contact time, strong solubility, The effect of increasing the yield
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Embodiment 1
[0021] Get the oxidized liquid (the azelaic acid content is about 70% of the 100kg oleic acid ozonation-oxidation reaction gained, the suberic acid content is about 3%, the palmitic acid and stearic acid content are about 10%, the pelargonic acid content is lower than 1.5%) ), put it in a rectification tower, and distill under reduced pressure under the conditions of 100-1000pa and 70-110°C to remove the C 2 -C 9 The monoacid, the residue is transferred to a thin film evaporator, distilled at 80pa, 190°C to remove heavy components such as asphalt; add the distilled crude azelaic acid to 500kg of water at a temperature of 60°C for extraction Operation, azelaic acid and other water-soluble substances dissolved in hot water, C 10-18 The saturated monocarboxylic acid is separated from the water layer, stirred, allowed to stand for stratification, and the upper oil layer is separated by overflow; the extracted water layer is extracted with 500kg aromatic hydrocarbons at a temperat...
example 2
[0023] Get 100kg oleic acid ozonation-oxidative decomposition gained oxidation solution (azelaic acid content is about 68%, suberic acid content is about 3.5%, palmitic acid and stearic acid content are about 12%, nonanoic acid content is less than 2%), Put it in a rectification tower for rectification, and distill under reduced pressure at 400-1200pa and 70-110°C to remove the C 2 ~C 9 Monoacid, transfer the residue to a thin film evaporator and distill at 140pa, 210°C to remove heavy components such as asphalt; add the distilled crude azelaic acid to 500kg of water at a temperature of 85°C, stir, and azelaic acid and other water-soluble substances dissolved in hot water, C 10-18 The saturated monocarboxylic acid is separated from the water layer, and the upper oil layer is separated after standing for stratification, and the extracted water layer is carried out with 500kg of aromatic hydrocarbons at a temperature of 85°C to carry out extraction, and the residual monoacid in...
example 3
[0025] Get 100kg of crude azelaic acid (azelaic acid content is about 70%, suberic acid content is about 3%, palmitic acid and stearic acid content are about 10%, pelargonic acid content is lower than 1.5%), it is placed in refining Distillation column rectification, vacuum distillation under the conditions of 800-2000pa, 90-150℃, to remove the C 2 ~C 9 Monoacid, transfer the residue to a thin film evaporator, distill at 140pa, 210°C to remove heavy components such as asphalt; add the distilled crude azelaic acid to 500kg of water at a temperature of 85°C for extraction , azelaic acid and other water-soluble substances dissolved in hot water, C 10-18 The saturated monocarboxylic acid is separated from the water layer, stirred, allowed to stand for stratification, and the upper oil layer is separated by overflow; the extracted water layer is extracted with 500kg aromatic hydrocarbons at a temperature of 85°C, and a small amount of monohydric acid remaining in the aqueous solut...
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