Silicon nitride composite ceramics heater
A technology of composite ceramics and silicon nitride, which is applied in the field of silicon nitride composite ceramic heating elements, can solve the problems that the point temperature difference range is not too wide, the thermal shock performance needs to be further improved, and the thermal conductivity of the heating element is not too high, so as to achieve the thermal conductivity Improvement, safe and reliable use, good thermal shock resistance
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[0006] Example 1-4:
[0007] (1) Preparation of raw materials: Weigh the ingredients according to the amount ratio in Table 1, and pass the vibrating ball mill for 8 hours, unload, sieving, baking at a constant temperature, and make wax cakes with wax, and keep them sealed.
[0008] (2) Preparation of blanks: processing metal molds according to the shape requirements of the heating element, and preparing blanks by hot die casting.
[0009] (2) Sintering: The prepared blank is loaded into the mold, furnace is loaded, dewaxed, hot pressed under the protection of flowing nitrogen, and the temperature is increased at a uniform rate. The sintering temperature is 1720±3°C; the pressure also slowly increases, and the pressure is controlled at 200- 250kg / cm 2 . After reaching the sintering temperature, the temperature is kept constant and the pressure is constant for 1 hour, and then the temperature is lowered and the pressure is maintained to 1550 ℃ when the power is cut off and the furn...
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