Rare earth doping metal halogenide photostimulable phosphor glass and preparation thereof
A metal halide and rare earth doping technology, which is applied in the field of rare earth doped metal halide-based luminescent phosphor glass and its preparation, can solve the problems of difficult control of material properties, many steps and procedures, and high production cost, and achieve Reduce the absorption of light signals, enhance the luminous intensity, and reduce the effects of external interference factors
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Embodiment 1
[0033] (1) First, vacuumize the glove box (Japan Sekisui Machinery Co., Ltd., MDB-2BL type), and control the vacuum degree of the glove box body to not be higher than 1×10 -1 Torr, saddlebag vacuum not higher than 5×10 -2 Torr, the oxygen content is below 100ppb, the moisture value is below 1.47ppb, then fill the glove box with nitrogen or argon with the same pressure as the surrounding atmosphere; then in the glove box, the molar percentage composition: 40 moles of AlF 3 -, 44.9 moles of BaF 2 , 5 M BaCl 2 , 10 moles of YF 3 , 0.1 mol EuF 3 , weighing a total of 20g of raw materials, the purity of the above-mentioned raw materials is not less than 99.95%, and the above-mentioned components are fully mixed and placed in a graphite crucible;
[0034] (2), the graphite crucible of above-mentioned charge is put into the small-scale high-frequency induction heating device (Japan Miwa Works, MU-1700C) that is placed in the glove box, heats up rapidly, simultaneously in the heat...
Embodiment 2
[0036] (1), the vacuum treatment of glove box is the same as embodiment 1, then in glove box by mole percentage composition: the AlF of 25 moles 3 -, 65 moles of BaF 2 , 1 M BaCl 2 , 8.5 moles of YF 3 , 0.5 mol EuF 3 , weighing a total of 20g of raw materials, the purity of the above-mentioned raw materials is not less than 99.95%, and the above-mentioned components are fully mixed and placed in a graphite crucible;
[0037] (2), the graphite crucible of above-mentioned charging is put into the small-sized high-frequency induction heating device identical with embodiment 1, heats up rapidly, feeds Cl in the heating chamber of high-frequency induction heating device simultaneously 2 Gas for atmosphere protection, where the flow rate of chlorine gas is 6ml / s, heated to 900 ° C and kept for 35 minutes, so that the raw materials are melted into liquid state, and then cooled to obtain rare earth doped metal halide system luminescent phosphor glass.
Embodiment 3
[0039] (1), the vacuum treatment of glove box is the same as embodiment 1, then in glove box by mole percentage composition: the AlF of 25 moles 3 , 40 M BaF 2 , 12 M BaCl 2 , 3 moles of SrBr 2 , 19 moles of YF 3 , 1 mol EuF 3 , weighing a total of 20g of raw materials, the purity of the above-mentioned raw materials is not less than 99.95%, and the above-mentioned components are fully mixed and placed in a graphite crucible;
[0040] (2), the graphite crucible of above-mentioned charging is put into the small-sized high-frequency induction heating device identical with embodiment 1, heats up rapidly, feeds Cl in the heating chamber of high-frequency induction heating device simultaneously 2 Gas for atmosphere protection, where the flow rate of chlorine gas is 15ml / s, heated to 950 ° C for 20 minutes, the raw materials are melted into a liquid state, and then cooled to obtain rare earth-doped metal halide system luminescent phosphor glass.
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