CdTeS/ZnS cladding quantum dot and preparation thereof
A quantum dot and cladding technology, which is applied in the field of CdTeS/ZnS cladding quantum dots and its preparation, can solve the problems of complex process, high price, and unsafety, and achieve the effects of high fluorescence intensity, low cost, and narrow half-peak width
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[0015] The preparation of CdTeS / ZnS quantum dots is divided into four parts: (a) preparation of Te and S stock solutions; (b) preparation of ZnO stock solutions; (c) synthesis of CdTeS / ZnS quantum dots; (d) post-treatment.
[0016] (a) Preparation of Te and S stock solutions
[0017] Add 5 mg Te powder and 320 mg S powder into a 25 ml round bottom flask (reactor A), transfer 5 ml OA and 1 ml TOP, and obtain TeS stock solution after dissolving.
[0018] (b) Add 163mg of ZnO into a 50ml three-neck flask (reactor B), transfer 5ml of OA and 20ml of TOA into it and stir evenly to prepare stock solution B.
[0019] (c) Synthesis of CdTeS quantum dots
[0020] A 100ml four-neck flask (reactor C) was equipped with stirring, a thermometer and an Ar gas protection device, accurately weighed 400 mg of CdO, added 20 ml of OA, 5 ml of TOA and 20 ml of TOP, replaced the clean air with Ar gas, and heated up while stirring. When the temperature of reactor C reaches 260-300°C, add stock solu...
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