Energy storage battery based on lithium ion conduction and preparation method (thereof)
A technology of an energy storage battery and a manufacturing method, applied in the field of electrochemistry, can solve the problems of high price of metal lithium materials, limited service life and safety, poor thermal stability, etc., and achieve excellent cycle performance, high energy density, and good safety performance. Effect
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Embodiment 1
[0019] First, add polyvinylidene fluoride to an appropriate amount of N-methylpyrrolidone, stir and dissolve to make a glue solution for use. The negative electrode active material Li 4 Ti 5 o 12 After mixing with carbon black, add it to the above glue (Li 4 Ti 5 o 12 : superconducting carbon black: mass percent of polyvinylidene fluoride=90:5:5), after fully stirring and mixing, evenly apply on both sides of aluminum foil (thickness is 20 μ m), make negative electrode sheet. Similarly, the positive electrode active material LiMn 2 o 4 After mixing with carbon black, add it to the above glue (LiMn 2 o 4 : carbon black: mass percent of polyvinylidene fluoride=92:5:3), after fully stirring and mixing, evenly apply on both sides of aluminum foil (thickness is 20 μ m), make positive electrode sheet.
[0020] The positive and negative electrode sheets prepared above were dried under vacuum at 80° C. for 8 hours, then rolled and cut. After the cut positive and negative ele...
Embodiment 2
[0023] First, polyvinylidene fluoride is added to an appropriate amount of N-methylpyrrolidone, stirred and dissolved to make a glue solution for use. The negative electrode active material Li 4 Ti 5 o 12 Mix with carbon black and add to the above glue (Li 4 Ti 5 o 12 : carbon black: mass percentage of polyvinylidene fluoride=75:15:10), after fully stirring and mixing, evenly apply on both sides of aluminum foil (thickness is 15 μ m), make negative pole sheet. Similarly, the positive electrode active material LiFePO 4 Mix with carbon black and add to the above glue (LiFePO 4 : carbon black: mass percent of polyvinylidene fluoride=80:12:8), after fully stirring and mixing, evenly apply on both sides of aluminum foil (thickness is 30 μ m), make positive electrode sheet.
[0024] The positive and negative electrode sheets prepared above were vacuum-dried at 80° C. for 6 h, rolled and punched. After the positive and negative plates are separated by a diaphragm, they are st...
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