Ultraviolet excitated red fluorescent powder surface treating method
A red fluorescent powder and surface treatment technology, applied in the direction of luminescent materials, chemical instruments and methods, etc., can solve the problems of large light attenuation, poor coating quality, uneven coating, etc., and achieve good luminescence and dispersion Effect
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Embodiment 1
[0014] (1), surfactant preparation: surfactant raw material γ—Al 2 o 3 Pass through a 400-mesh sieve, remove the sieve residue on the 400-mesh sieve, put the rest of the powder into a ball mill bottle, and ball mill for 12-48 hours with a ratio of powder: ball: water of 1:2:2 according to the mass percentage, and then ball mill Pass the obtained solution through a 600-mesh sieve, adjust the concentration of the solution and stir the solution at a high speed for 12-24 hours to obtain a surfactant, which is γ-Al with a mass percentage concentration of 20%. 2 o 3 solution, here the dispersing ball is required to be 0.5—1.5mm agate ball;
[0015] (2), yttrium oxide europium red fluorescent powder pretreatment: yttrium oxide europium red fluorescent powder slurry treatment, through 500 mesh sieve, remove the sieve residue on the 500 mesh sieve, the powder slurry that all the other obtains is qualified powder slurry, will Qualified powder slurry is washed 2-5 times with water; ...
Embodiment 2
[0018] (1), surfactant preparation: surfactant raw material γ—Al 2 o 3 Pass through a 400-mesh sieve, remove the sieve residue on the 400-mesh sieve, put the rest of the powder into a ball mill bottle, and ball mill for 12-48 hours with a ratio of powder: ball: water of 1:2:2 according to the mass percentage, and then ball mill Pass the obtained solution through a 600-mesh sieve, adjust the concentration of the solution and stir the solution at a high speed for 12-24 hours to obtain a surfactant, which is γ-Al with a mass percentage concentration of 20%. 2 o 3 solution, here the dispersing ball is required to be 0.5—1.5mm agate ball;
[0019] (2), yttrium oxide europium red fluorescent powder pretreatment: yttrium oxide europium red fluorescent powder slurry treatment, through 500 mesh sieve, remove the sieve residue on the 500 mesh sieve, the powder slurry that all the other obtains is qualified powder slurry, will Qualified powder slurry is washed 2-5 times with water; ...
Embodiment 3
[0022] (1), surfactant preparation: surfactant raw material γ—Al 2 o 3 Pass through a 400-mesh sieve, remove the sieve residue on the 400-mesh sieve, put the rest of the powder into a ball mill bottle, and ball mill for 12-48 hours with a ratio of powder: ball: water of 1:2:2 according to the mass percentage, and then ball mill Pass the obtained solution through a 600-mesh sieve, adjust the concentration of the solution and stir the solution at a high speed for 12-24 hours to obtain a surfactant, which is γ-Al with a mass percentage concentration of 20%. 2 o 3 solution, here the dispersing ball is required to be 0.5—1.5mm agate ball;
[0023] (2), yttrium oxide europium red fluorescent powder pretreatment: yttrium oxide europium red fluorescent powder slurry treatment, through 500 mesh sieve, remove the sieve residue on the 500 mesh sieve, the powder slurry that all the other obtains is qualified powder slurry, will Qualified powder slurry is washed 2-5 times with water; ...
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