High temperature resistant surface-insulated FeCrAl electrothermal alloy and preparation method thereof
An electrothermal alloy, high temperature resistant technology, applied in heating element materials, metal material coating process, solid-state chemical plating, etc.
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Embodiment 1
[0014] Embodiment 1, high temperature resistant surface insulating FeCrAl electrothermal alloy, characterized in that: a high temperature resistant and insulating composite alumina protective layer containing rare earth is set on the FeCrAl electrothermal alloy substrate.
[0015] The preparation method provided by the present invention is as follows: first, the FeCrAl electrothermal alloy product is degreased and derusted, and then rinsed; secondly, the rinsed product is immersed in a sol-gel containing rare earth, and it is taken out and dried after about 10 minutes. ; Finally, between 850-950 ° C in a protective atmosphere for about 180 minutes of heat treatment to obtain a FeCrAl electric heating alloy product with high temperature resistant surface insulation.
Embodiment 2
[0016] Embodiment 2. The preparation method provided by the present invention is as follows: first, rinse the FeCrAl electrothermal alloy product after degreasing and rust removal treatment; secondly, immerse the rinsed product in the sol-gel body containing rare earth for about 20 minutes Then take it out and dry it; finally heat treatment at 850-950°C in a protective atmosphere for about 120 minutes to obtain a FeCrAl electric heating alloy product with high temperature resistant surface insulation.
Embodiment 3
[0017] Embodiment 3. The preparation method provided by the present invention is as follows: firstly, rinse the FeCrAl electrothermal alloy product after degreasing and derusting treatment; secondly, immerse the rinsed product in a solution containing 1-5% hydrated aluminum hydroxide, 5 / 10,000 cerium-containing rare earth compound sol-gel body, take it out and dry it after about 16 minutes; finally heat treatment at 850-950°C in a protective atmosphere for about 160 minutes to obtain a high temperature resistant surface insulation FeCrAl electric heating alloy products.
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