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Method for preparing mulberry cigarette flavor

A technology of spices and mulberries used in cigarettes, which is applied in the field of tobacco in the cigarette industry, can solve the problems of difficult removal of pectin carbohydrates, affect the sensory quality of cigarettes, and increase the stimulation of cigarette smoke, so as to facilitate production transformation, improve cigarette quality, Overcomes residual and irritating effects

Inactive Publication Date: 2009-11-04
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The main reason is that mulberry contains a lot of pectin, tannin, tannin and other ingredients, which are not good for the aroma of tobacco, which will increase the stimulation of cigarette smoke, and also bring oral residues and unclean aftertaste, which seriously affect the taste of cigarettes. sensory quality
In addition, mulberry also contains a large amount of carbohydrates, including monosaccharides, disaccharides and polysaccharides. Excessive carbohydrates added to cigarettes will lead to dry smoke and increased CO concentration
[0006] In the prior art, the extraction of active ingredients in mulberries mainly adopts conventional solvent extraction methods, which can obtain most of the nutrients in mulberries, but it contains a large amount of pectin and carbohydrates and other ingredients that are not conducive to cigarette smoke
Pectin, tannins, tannins, and excess carbohydrates are difficult to remove by traditional solvent extraction

Method used

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  • Method for preparing mulberry cigarette flavor
  • Method for preparing mulberry cigarette flavor
  • Method for preparing mulberry cigarette flavor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Embodiment 1. Get the dried fruit of mulberry fruit, rinse thoroughly by flotation, put into oven after constant temperature (60 ℃) dry 8h (moisture control is at about 5%), pulverize and cross 20 mesh sieves. Weigh 100g, add 400g of 75% edible alcohol to soak overnight, distill and extract twice, each time for 4h, the extraction temperature is 85°C. Combine the extracts, let stand, settle naturally for 2 days, add 1 times the amount of petroleum ether for extraction, remove the petroleum ether phase (to basically no residue), concentrate into mulberry water extract, and pass the mulberry water extract through the pretreated macropores Resin D101, rinse with 70% alcohol to obtain mulberry eluate, add 10% propylene glycol in the mulberry eluent, then concentrate it to a bomm degree of 20 to obtain mulberry extract, combine mulberry extract with alcohol solvent After mixing at a ratio of 1:9, the mulberry tobacco flavor is obtained.

Embodiment 2

[0037] Embodiment 2. Get the dried mulberry fruit, rinse it with tap water, put it into an oven at a constant temperature (60° C.) and dry it for 8 hours (moisture is controlled at about 5%), and pulverize through a 20-mesh sieve. Weigh 100g, add 500g of 75% edible alcohol to soak overnight, distill and extract twice, the first time is 4h, the second time is 3h, the extraction temperature is 85°C. Combine the extracts, let stand and settle for 3 days, add 1 times the amount of n-hexane for extraction, remove the n-hexane phase (to basically no residue), concentrate into mulberry water extract, pass the mulberry water extract through the pretreated macroporous resin D140, Rinse with 65% alcohol to obtain the mulberry eluate, add 10% propylene glycol to the mulberry eluate, then concentrate it to a bomm degree of 20 to obtain the mulberry extract, and mix the mulberry extract and the alcohol solvent in a ratio of 1:9 After mixing in the ratio of mulberry tobacco flavoring is obt...

Embodiment 3

[0038] Embodiment 3. Get the dried fruit of mulberry fruit, rinse it with tap water, put it into an oven at a constant temperature (60° C.) and dry it for 8 hours (moisture is controlled at about 5%), and pulverize through a 20 mesh sieve. Weigh 100g, add 400g of 70% edible alcohol to soak overnight, distill and extract twice, each 4h, extraction temperature 85°C. Combine the extracts, let stand for 2 days, add 1 times the amount of pentane for extraction, remove the pentane phase (to basically no residue), concentrate into mulberry water extract, pass the mulberry water extract through the pretreated macroporous resin D101, Rinse with 65% alcohol to obtain the mulberry eluate, add 10% propylene glycol in the mulberry eluent, then concentrate to 20 bomidoness to obtain the mulberry extract, the mulberry extract and the alcohol solvent in a ratio of 1:9 After mixing in proportion, the mulberry tobacco flavor is obtained.

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Abstract

The invention discloses a method for preparing a mulberry cigarette flavor, belonging to the technical field of cigarette in the cigarette industry as well as a preparation method of essence and flavors. The method comprises the following steps: (1), preparing materials: bleaching, floating, drying and crushing dried mulberry fruits and screening with a net of 10 to 100 meshes to obtain mulberry powder; (2), extracting: distilling and extracting the mulberry powder, screening with millipores and keeping filtrate; (3), extracting and concentrating to obtain paste as an aqueous mulberry extract;(4), absorbing with macroporous resin to obtain mulberry eluate; (5), reducing pressure and concentrating to obtain a mulberry extract; and (6), preparing the flavor: mixing the mulberry extract and alcohol according to a proportion to obtain a solution as the mulberry cigarette flavor. The method has the following advantages of simple technology, active ingredient maintenance, strong stability of the prepared mulberry cigarette flavor, clean buccal aftertaste, good compatibility with cigarette smell, no residue and low cost.

Description

technical field [0001] The invention belongs to the technical field of tobacco in the cigarette industry, and relates to a method for preparing essence and fragrance, in particular to a method for preparing tobacco fragrance from natural plant fruit mulberry. Background technique [0002] At present, the application of natural plant extracts as additives in cigarette flavoring has become one of the key points and hot spots in the development of the tobacco industry. As the coke-reducing effect of Chinese herbal medicine additives in cigarettes is increasingly accepted by consumers, more and more tobacco researchers are looking for tobacco flavors and fragrances from natural Chinese herbal medicines, and the application of natural flavors in cigarette flavor blending more and more widely. [0003] Mulberry is the mature aggregate fruit of the deciduous tree Mulberry (Morusalba L.), also known as mulberry, which is composed of many small achenes. Mulberry is rich in nutrient...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/18A24B15/24
Inventor 程华丁碧军熊斌熊国玺朱巍李丹
Owner HUBEI CHINA TOBACCO IND
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