Optical conversion luminous film and preparation method thereof
A technology of luminescent film and light conversion, applied in luminescent materials, luminescent coatings, chemical instruments and methods, etc., can solve the problem of large-area uniformity and consistency of luminescent materials, no mention of manufacturing luminescent films, and no uniform light effect And other issues
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Embodiment 1
[0049] Example 1: Application method one to manufacture light-converting luminescent film
[0050] The process recipe for the manufacture of the mixed paint layer is as follows:
[0051] Resin Silicone resin 88.949kg
[0052] Bisaminosilane N-β-(aminoethyl)-γ-aminopropylmethyltrimethoxysilane 1.000kg
[0053] Auxiliary defoamer 0.050kg
[0054] yellow luminescent fluorescent material
[0055] 0.45Tb 2 o 3 0.9Al 2 o 3 0.1Ga 2 o 3 : 0.004Ce, 0.004Li, 0.2F 10.000kg
[0056] Red luminescent fluorescent material 2-Juronidinyl-3-hydroxyflavone 0.001kg
[0057] Implementation process: Add the liquid raw materials in the formula into the batching container, stir evenly, slowly add the fluorescent material into the container at high speed, disperse evenly, and set aside. Of which 0.45Tb 2 o 3 0.9Al 2 o 3 0.1Ga 2 o 3 : 0.004Ce, 0.004Li, 0.2F particle size is 8μm, 2-juronidinyl-3-hydroxyflavone particle size is 3μm. The prepared mixed paint is coated on the corona-treat...
Embodiment 2
[0059] Embodiment 2: Manufacture light conversion luminescent film by method one
[0060] The process formula of the mixed coating layer is as follows:
[0061] Resin Polyurethane resin sap 60.000kg
[0062] Yellow-emitting fluorescent material (Sr 0.5 Ca 0.5 ) 1.95 Si 5 N 8 :Eu 0.05 , Li 0.05 , F 0.1 17.500kg
[0063] Red-emitting fluorescent materials (Sr0.1 Ca 0.9 ) 1.99 Si 5 N 8 :Eu 0.01 , Li 0.1 , F 0.01 0.500kg
[0064] Thinner Cyclohexanone 20.000kg
[0065] Bisaminosilane 3-piperazinylpropylmethyldimethoxysilane 1.000kg
[0066] Auxiliary leveling agent EFKA-30 0.500kg
[0067] Defoamer EFKA-21 0.500kg
[0068] Weigh the raw materials according to the formula, add the liquid raw materials in the formula into a high-speed disperser, disperse evenly at high speed, then add fluorescent materials and stir evenly, wherein (Sr 0.5 Ca 0.5 ) 1.95 Si 5 N 8 :Eu 0.05 , Li 0.05 , F 0.1 The particle size is 15μm, (Sr 0.1 Ca 0.9 ) ...
Embodiment 3
[0069] Embodiment 3: Application Method 1 to manufacture light-converting luminescent film.
[0070] The process formula of the mixed coating layer is as follows:
[0071] Resin Urethane resin 50.000kg
[0072] Urethane resin curing agent 5.000kg
[0073] Bisaminosilane N-β-(aminoethyl)-γ-aminopropylmethyldimethoxysilane 5.000kg
[0075] yellow luminescent fluorescent material
[0076] 0.95CaO 0.05SrO 0.4MgO SiO 2 :0.015Eu, 0.005Li, 0.25F 30.000kg
[0077] Red-emitting fluorescent materials (Sr 0.1 Ca 0.9 ) 1.99 Si 5 N 8 :Eu 0.01 , Li 0.1 , F 0.01 2.000kg
[0078] Weigh the raw materials according to the formula, add the liquid raw materials in the formula into the high-speed disperser, disperse evenly at high speed, then add fluorescent materials and stir evenly, of which 0.95CaO·0.05SrO·0.4MgO·SiO 2 : 0.015Eu, 0.005Li, 0.25F particle size is 10μm, (Sr 0.1 Ca 0.9 ) 1.99 Si 5 N 8 :Eu 0.01 , Li 0.1 , F 0.01 ...
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