Polyvinyl acetate mixed suspended liquid and preparation method and application thereof
A technology of polyvinyl acetate and vinyl acetate, which is applied in the field of polyvinyl acetate suspension and its preparation and application, can solve the problems of poor stability and high vinyl acetate monomer, and achieve good suspension and settlement performance , Low requirements for production equipment, good stability
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[0042] Example 1
[0043]
[0044]
[0045] After pre-filled with nitrogen, a reactor equipped with a stirrer, a reflux condenser and a thermometer is added stabilizer and water, and dissolved. Add 20% of vinyl acetate, start stirring, heat the thermostat, and control the reaction temperature at 70°C. Take the initiator and add 1 / 3 of its mass into the reactor. After starting the reaction, add the remaining 80% of vinyl acetate and the remaining 2 / 3 of the initiator dropwise, and the drop will be finished within 3 hours. Continue the reaction for about 3 hours until there is no reflux. After the material was cooled to 50°C, 1% sodium bicarbonate solution was added to adjust the pH of the material to 5. A white opaque emulsion is obtained, and the solid content of the material is adjusted to about 30% with purified water, which is a medicinal polyvinyl acetate suspension.
[0046] The content of each component of the polyvinyl acetate suspension is as follows:
[0047]
Example Embodiment
[0048] Example 2
[0049]
[0050]
[0051] After pre-filled with nitrogen, a reactor equipped with a stirrer, a reflux condenser and a thermometer is added stabilizer and water to dissolve. Add 40% of vinyl acetate, start stirring, heat the thermostat, and control the reaction temperature at 65°C. Take the initiator and add 2 / 5 of its mass to the reactor. After starting the reaction, add the remaining 60% of vinyl acetate and the remaining 3 / 5 of the initiator dropwise, and the drop will be finished within 3 hours. Continue the reaction for about 3 hours until there is no reflux. After the material was cooled to 50°C, 1% sodium bicarbonate solution was added to adjust the pH of the material to 4. A white opaque emulsion is obtained, and the solid content of the material is adjusted to about 30% with purified water, which is a medicinal polyvinyl acetate suspension.
[0052] The content of each component of the polyvinyl acetate suspension is as follows:
[0053]
Example Embodiment
[0054] Example 3
[0055]
[0056] After pre-filled with nitrogen, a reactor equipped with a stirrer, a reflux condenser and a thermometer is added stabilizer and water to dissolve. Add 28% of vinyl acetate, start stirring, heat the thermostat, and control the reaction temperature at 75°C. Take the initiator and add 1 / 3 of its mass to the reactor. After starting the reaction, add the remaining 72% of vinyl acetate and the remaining 2 / 3 of the initiator dropwise, and the drop will be finished within 3 hours. Continue the reaction for about 3 hours until there is no reflux. After the material was cooled to 50°C, 1% sodium bicarbonate solution was added to adjust the pH of the material to 6. A white opaque emulsion is obtained, and the solid content of the material is adjusted to about 30% with purified water, which is a medicinal polyvinyl acetate suspension.
[0057] The content of each component of the polyvinyl acetate suspension is as follows:
[0058]
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