High heat-resistance organic solder ability preservative
A kind of solder protection agent, organic technology, applied in the field of high heat resistance organic solder protection agent, to achieve the effect of improving solderability, inhibiting oxidation, and excellent tinning
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Embodiment 1~12
[0039] In Examples 1 to 12, except that the contents of imidazole compounds and aromatic phenol oxygen absorbers are as listed in Table 1, the composition of the high heat-resistant organic soldering flux is as follows: the content of acetic acid is 15.6%, The content of isopropanol is 1.2%, copper chloride is 0.1%, zinc acetate is 0.05%, and the balance is deionized water.
[0040] Preparation method: Add 2-carboxy-1-phenol and acetic acid into a clean enamel stirring tank at room temperature, add 5-chloro-2-benzylbenzimidazole during the stirring process, and after stirring for half an hour, the solid substance is basically Dissolve completely above, then add deionized water, isopropanol, copper chloride and zinc acetate in sequence, continue to stir for one hour until the solid raw materials are completely dissolved, mix evenly, stop stirring, stand and filter, and obtain a solution with a pH value of 3.40. Heat-resistant organic flux products. If the pH is lower than 2.5 ...
Embodiment 13~18
[0051] In Examples 13-18, except that the aromatic phenolic oxygen absorber content is listed in Table 2 in the composition of the high heat-resistant organic flux, the other components are: 3-chloro-2-benzylbenzimidazole 0.36%, the content of acetic acid is 15.6%, the content of isopropanol is 1.2%, copper chloride is 0.1%, zinc acetate is 0.05%, and the balance is deionized water.
[0052] Preparation method is identical with embodiment 1~12.
[0053] Table 2 is a comparison of the results of the tin test on the through hole of the weldment using the high heat-resistant organic fluxes of Examples 13-18 and the heat-resistant organic fluxes of Comparative Examples 4 and 5:
[0054] The high heat-resistant organic fluxes of Comparative Examples 4 and 5 are all prepared from imidazole compounds, organic acids, solubilizers, metal compounds, and deionized water, and do not contain aromatic phenol oxygen absorbers.
[0055] A copper-clad laminate base material with a length, wid...
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