Check patentability & draft patents in minutes with Patsnap Eureka AI!

Method for refining cosmetic camellia oil by adopting short-path distillation

A short-path distillation, cosmetic-grade technology, applied in the direction of oil/fat refining, fat production, etc., can solve the problems of large loss of camellia oil, secondary pollution, and more oil wasted, and achieve the goal of reducing implementation costs and avoiding secondary pollution. Effect

Inactive Publication Date: 2010-06-02
SOUTH CHINA UNIV OF TECH
View PDF1 Cites 24 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] (1) The loss of camellia oil is large, and one part of oil is lost for one part of acid removal, and more oil is lost
[0005] (2) Separating the neutralized substance (sodium soap) is usually separated by high-speed centrifugation, washed with water and then dried; the separated sodium soap and water are easy to cause secondary pollution if not handled properly
[0006] (3) The above general method deacidification process loses high value-added oleic acid

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for refining cosmetic camellia oil by adopting short-path distillation
  • Method for refining cosmetic camellia oil by adopting short-path distillation
  • Method for refining cosmetic camellia oil by adopting short-path distillation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] (1) Weighing a certain pressed camellia oil crude oil 10Kg, its measurement acid value AV is 8mgKOH / g; This pressed camellia oil crude oil directly enters buffer tank 1 place, is imported into the first stage film evaporator 2 by metering pump Dehydration and degassing are carried out at a temperature of 80°C and a pressure of -0.9Mpa. After dehydration and degassing, the pressed camellia oil continues to enter the next short-path distiller for deacidification and separation.

[0034] (2) The pressed camellia oil after dehydration and degassing is imported into the second-stage short-path distiller 3 through a pump to carry out deacidification and separation. Sour camellia oil.

[0035] (3) The pressed camellia oil after deacidification is pumped into the third-stage short-path distiller 4 for further deacidification and separation. The specific conditions are that the distillation temperature is 180° C. and the pressure is 0.1 Pa for separation.

[0036] The free fat...

Embodiment 2

[0038] (1) Weighing 10Kg of camellia oil crude oil extracted by a certain solvent, its measurement acid value AV is 6mgKOH / g, the camellia oil extracted by this solvent directly enters buffer tank 1, and is imported into the first-stage thin film evaporator by metering pump 2. Carry out dehydration and degassing, specifically at a temperature of 120°C and a pressure of -0.8Mpa. The solvent-extracted camellia oil after dehydration and degassing continues to enter the next short-path distiller for deacidification and separation.

[0039] (2) The solvent-extracted camellia oil after dehydration and degassing is input into the second-stage short-path distiller 3 through a pump to carry out deacidification and separation. Oil.

[0040] (3) The solvent-extracted camellia oil after deacidification is pumped into the third-stage short-path distiller 4 for further deacidification and separation. The specific conditions are that the distillation temperature is 170° C. and the pressure ...

Embodiment 3

[0043](1) Weigh 10Kg of pressed camellia oil from Huiying camellia oil factory in Hengyang, Hunan, and its measured acid value AV is 6.5mgKOH / g, and the camellia oil extracted by this solvent is directly put into buffer tank 1, and is input to the first stage by metering pump The thin film evaporator 2 performs dehydration and degassing, specifically at a temperature of 100°C and a pressure of -0.85Mpa. The solvent-extracted camellia oil after dehydration and degassing continues to enter the next short-path distiller for deacidification and separation.

[0044] (2) The solvent extracted camellia oil after dehydration and degassing is pumped into the second-stage short-path still 3 for deacidification and separation. The specific conditions are that the distillation temperature is 130° C. and the pressure is 5 Pa to separate the deacidification camellia oil .

[0045] (3) The solvent-extracted camellia oil after deacidification is pumped into the third-stage short-path distill...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Acid valueaaaaaaaaaa
Acid valueaaaaaaaaaa
Acid valueaaaaaaaaaa
Login to View More

Abstract

The invention discloses a method for refining cosmetic camellia oil by adopting short-path distillation, which is characterized by adopting a first-stage film distillator and a second-stage short-path evaporator to carry out deacidification on crude camellia oil. In the step of first-stage film distillation, dehydration and removal of the substances with low boiling point are carried out, in the step of second-stage distillation, removal of free fatty oil is carried out on the camellia oil processed on the first stage and in the step of third-stage distillation, removal of free fatty oil is carried out on the camellia oil processed on the second stage. The three-stage distillation is carried out under the conditions of working temperatures controlled between 60 DEG C and 180 DEG C and the pressure between minus 0.6MPa and 0.1Pa, and oleic acid with high acid value and camellia oil with ultralow acid value are obtained. The process with high pollution of wastewater drained after soda soap washing and water washing in the chemical processes of alkali refining and neutralizing does not exist during processing the camellia oil. The flow is simple, the oleic acid with high value and the camellia oil with ultralow acid value are separated by distillation, the separation process is a physical process, and the camellia oil is free of loss, thus having very high yield.

Description

technical field [0001] The invention relates to a method for refining cosmetic-grade camellia oil by means of a short-path still. It specifically relates to a treatment method for separating high-quality camellia oil with ultra-low acid value by using short-distance distillation technology, which meets the national cosmetic grade low-acid value camellia oil standard; it belongs to the field of deep processing of natural products and agricultural by-product processing. Background technique [0002] Camellia oil is an important daily oil and industrial raw material. Such as figure 1 As shown, the current general method of deacidification of camellia oil is to use alkali to neutralize (called alkali refining) camellia oil crude oil and then make it by static sedimentation or centrifugal separation, water washing and standing still sedimentation or centrifugal separation and drying and dehydration again Deacidified camellia oil. [0003] Chinese invention patent application C...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C11B3/12
Inventor 朱宝璋朱力
Owner SOUTH CHINA UNIV OF TECH
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2025 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com