Polymer composite material with oriented padding and preparation method thereof
A composite material and polymer technology, applied in the field of polymer composite materials and its preparation, can solve the problems of cumbersome process, time-consuming, difficult large-scale production, etc., and achieve the effect of simple equipment, common raw materials, and outstanding substantive characteristics
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[0044] Example 1
[0045] The polymer composite material with oriented filler comprises a polymer matrix filled with a filler with shape anisotropy. In this embodiment, the polymer matrix is polyvinyl alcohol (PVA) with a molecular weight of about 7000, and the filler is Na-type montmorillonite. The material composed of polyvinyl alcohol (PVA) and Na-type montmorillonite is prepared into a composite material by a layer-multiplier extrusion method of segmentation-restacking and confluence, and the anisotropic filler is oriented in the material flow during the preparation.
[0046] The preparation method of the polymer composite material with oriented filler includes:
[0047] Preliminary steps: Put an appropriate amount of montmorillonite powder into deionized water, then vigorously stir for a period of time (for example, two weeks), then let it stand, and then collect the supernatant after the rest. PVA was slowly added to 80°C deionized water, and dissolved under vigorous stirri...
Example Embodiment
[0050] Example 2
[0051] The polymer composite material with oriented filler adopts a dual structure, that is, two different materials are laminated and then extruded. It includes two polymer matrices, and the first polymer matrix is filled with a shape-anisotropic filler. In this embodiment, the first polymer matrix is polycarbonate (PC), the second polymer matrix is polyethylene terephthalate (PET), and both PC and PET are commercially available products. . The polycarbonate (PC) is filled with a filler. The filler is talc. The average thickness of the talc particles is about 2 microns, and the aspect ratio is about 10, that is, the average diameter is about 20 microns. The aforementioned polycarbonate (PC) and talc constitute material composition A, and the PET constitute material composition B. The composition of these materials is prepared into a composite material by a layer multiplication extrusion method of lamination-segmentation-layering and confluence, and th...
Example Embodiment
[0055] Example 3
[0056] The polymer composite material with oriented filler comprises a polymer matrix filled with a filler with shape anisotropy. In this embodiment, the polymer matrix is nylon 6, the filler is organic montmorillonite, and the organic montmorillonite is a clay modified by intercalation of 12 amino acids and 12 acids. The material composed of nylon 6 and organic montmorillonite is prepared into a composite material by a layer-multiplier extrusion method of segmentation-restacking and confluence. During the preparation, the shape anisotropic filler is oriented in the material stream.
[0057] The preparation method of the polymer composite material with oriented filler includes:
[0058] Preliminary steps: first mix caprolactam with organic montmorillonite, and then use in-situ wet polymerization to prepare a 5wt% exfoliated clay-filled nylon 6 nanocomposite (the montmorillonite is almost completely exfoliated in the nylon 6 matrix), crush Composite materials.
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