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71results about How to "Easy to get equipment" patented technology

6-amino-6-deoxyinulin as well as preparation and application thereof

The invention relates to fields of daily chemicals and pharmaceuticals industry, in particular to 6-amino-6-deoxyinulin as well as preparation and application thereof. In the 6-amino-6-deoxyinulin shown as a formula (I), the average value range of n is 10-35. The preparation comprises the steps of undergoing a helogenation reaction of inulin or undergoing esterification of inulin and sulfonyl chloride, respectively undergoing a reaction of the product obtained through the helogenation reaction of the inulin or the esterification and sodium azide or azido lithium at a temperature of 40-70 DEG C for 8-24 hours to obtain 6-azido-6-deoxyinulin, and reducing the 6-azido-6-deoxyinulin by utilizing triphenylphosphine or lithium aluminium hydride to obtain the 6-amino-6-deoxyinulin. In the invention, the 6-amino-6-deoxyinulin is obtained through an effective synthetic means; an inulin six-position easily-leaving group is obtained through utilizing halogen to substitute the primary hydroxyl ofthe inulin or through the esterification of inulin and sulfonyl chloride; and the 6-amino-6-deoxyinulin with high substitution is obtained through azido nucleophilic substitution and reduction. The 6-amino-6-deoxyinulin synthesized by the preparation method provided by the invention is simple in the synthetic step and easy to popularize; and the required equipment and raw materials are easy to get. The formula (I) is shown in the specification.
Owner:YANTAI INST OF COASTAL ZONE RES CHINESE ACAD OF SCI

Preparation method of high-strength super-hydrophobic paper on the basis of layer by layer self-assembly and thermal induction treatment

ActiveCN107503228ASuperior superhydrophobic propertiesSimple equipment and operationFlexible coversWrappersIonINDUCTION TREATMENT
The invention relates to a preparation method of high-strength super-hydrophobic paper on the basis of layer by layer self-assembly and thermal induction treatment, and belongs to the technical field of post-processing of paper. The preparation method includes the steps of: 1) soaking common paper in a chitosan solution being 2-3 g/L in concentration for 10-20 min, moving the paper out, and washing the paper in deionized water for 3-5 times, and drying the paper for 10-20 min at 60-80 DEG C; 2) soaking the processed paper in a hexadecyl trimethoxysilane graft-modified nano TiO2-ethanol solution for 10-20 min, moving the paper out, and washing the paper in deionized water for 3-5 times, and drying the paper for 10-20 min at 60-80 DEG C, wherein the concentration of the hexadecyl trimethoxysilane graft-modified nano TiO2-ethanol solution is 2-4 g/L; 3) repeating the steps 1) and 2) for 20-30 times, and finally processing the treated paper for 20-30 min at 140-160 DEG C to form the high-strength super-hydrophobic paper. The preparation method is simple and employs simple equipment, overcomes the defects that preparation methods of super-hydrophobic paper in the prior art are complex in steps and need complex and expensive equipment. The preparation method is suitable for industrial production.
Owner:KUNMING UNIV OF SCI & TECH

Secret sea cucumber preparation method capable of removing fish smell at low temperature

The invention belongs to the technical field of seafood processing, and relates to a secret sea cucumber preparation method capable of removing fish smell at low temperature. The method comprises the six steps of processing fresh sea cucumber, removing the fish smell of the sea cucumber, blending traditional Chinese medicines, decocting yellow rice wine medicine soup, secretly making the sea cucumber and carrying out freeze drying; the method concretely comprises the steps of processing the fresh sea cucumber for later use, feeding ferment liquid into water to prepare fish smell removal liquid, and soaking the sea cucumber into the fish smell removal liquid to remove the fish smell; blending all the traditional Chinese medicines in proportion, and decocting the yellow rice wine medicine soup by yellow rice wine; putting the sea cucumber into the yellow rice wine medicine soup, and secretly making the sea cucumber; and finally, carrying out cold drying by a freeze drying device to obtain the sea cucumber finished product with the fish smell removed at low temperature. The preparation method has the advantages that preparation technology is simple and equipment is easily available; the sea cucumber finished product is rich in nutrition, good in low-temperature fish smell removal effect, obvious in health care and health maintenance effects, good in mouth feel and friendly to edible environment.
Owner:QINGDAO JINGUYUAN LIFE TECH

Amphiphilic amido inulin and preparation method thereof

The invention relates to the field of daily chemicals and the medicine industry, in particular to an amphiphilic amido inulin and a preparation method thereof. The amphiphilic amido inulin is shown in a formula (1), wherein R is H, CH3, CH3CH2CH2, (CH3)2CH or C6H5; and the average numeric area of n is 10-35. The preparation method comprises the following steps of: performing halogenating reaction on the primary hydroxyl of inulin; after reaction, reacting with sodium azide or lithium azide at 40-70 DEG C for 8-24 hours; purifying to obtain 6 azide-3,4-succinate-6 deoxidized inulin; and reducing the 6 azide-3,4-succinate-6 deoxidized inulin by utilizing triphenylphosphine, so as to obtain the amphiphilic amido inulin. According to the pepaation method, the amphiphilic amido inulin is obtained by virtue of an effective synthesis means, halogen is used for replacing the primary hydroxyl of inulin so as to cause that the sixth-site group of the inulin is ionized easily, acyl is used for protecting the naked hydroxy, at the othe sites, of the inulin, azido is used for performing nucleophilic substitution on the sixth-site group which is ionized easily, and the product is reduced so as to obtain the amphiphilic amido inulin with high substitution degree. The preparation method has the advantages that the synthesis step is simple, popularization is easy, and required equipment and raw materials are easily available. The formula (1) is shown in the specification.
Owner:YANTAI INST OF COASTAL ZONE RES CHINESE ACAD OF SCI

Free-water-surface cascaded ecological wetland and water purification method thereof

InactiveCN110143721ALandscape with great potentialRemoval of functional divisionsWater contaminantsMultistage water/sewage treatmentPurification methodsEmergent plant
The invention relates to a free-water-surface cascaded ecological wetland and a water purification method thereof. The free-water-surface cascaded ecological wetland comprises a bank slope, and further comprises a synchronous nitrification-denitrification functional zone, an aquatic plant pollution-reducing functional zone, a porous medium filter bed filtration and phosphorus removal functional zone and a submerged plant ecological diversity restoration functional zone sequentially arranged along a water flow direction. The water inlet of the free-water-surface cascaded ecological wetland is provided with a wetland water inlet weir plate, and the effluent outlet of the free-water-surface cascaded ecological wetland is provided with a wetland effluent weir plate; the bank slope is providedwith an ecological slope protection structure with a slope of no more than 1 / 3; and the ecological slope protection structure comprises submerged plants, emergent plants and terrestrial plant belts planted from the bottom of the slope to the top of the slope. The functional zones of the free-water-surface cascaded ecological wetland in the invention are specially designed and constructed accordingto the requirements of water purification, so organic matters, suspended matters and nitrogen and phosphorus nutrients are effectively removed; COD, NH3-N and TP in wetland effluent meets requirements on class-IV water quality; the concentration of TN is less than 10 mg / L; and the wetland effluent meets requirements on general landscape water and has the same biodiversity index as general landscape water.
Owner:SOUTHEAST UNIV

High-damping Mg-based damping alloy and preparation method thereof

The invention discloses a high-damping Mg-based damping alloy and a preparation method thereof. The alloy comprises 1-5% of Cu, 1-3% of Mn, 1-4% of Zn, 1-2% of Si, 0.1-0.5% of Ti, and the balance Fe. The method comprises the following steps: carrying out solid solution treatment on a melted alloy material at 300-400DEG C, carrying out heat insulation for 3-6h, carrying out water quenching to room temperature, ageing at 120-190DEG C, carrying out heat insulation for 25-30h, and carrying out air cooling to room temperature in order to obtain the Mg-based damping alloy. Melting in protection atmosphere is carried out, then casting is carried out, and finally heat treatment is carried out. The Mg-based damping alloy obtained in the invention can successfully solve the contradiction of the strength and the damping performance of a magnesium alloy, has the advantages of simple method and easily available equipment, and is suitable for large-scale industrial production. Ti, Mn and Cu are introduced on the basis of alloy element kind and content optimization in order to realize solid solution reinforcement and precipitation reinforcement. The orientation of a precipitated phase is adjusted by refining the crystal grain size in order to increase the strength and the plasticity of the above material. The tensile strength, the yield strength and the elongation of the Mg-based damping alloy are 360-420MPa, 260-290MPa and ~9% respectively. The magnesium alloy obtained in the invention can be obtained through routine casting molding, and the specific damping capacity of the magnesium alloy can reach 46-54%.
Owner:曹帅

Smart phone-based multi-media teaching approach

The invention brings forward a smart phone-based multi-media teaching approach. A projector screen (1), a smart phone (2), a program unit (3), a computer (4), a teaching material key point unit (5), a teacher unit (6), and a microphone (7) are arranged. The program unit (3) is installed in the smart phone (2) and the computer (4); and the teaching material unit opened by the teacher unit (6) and displayed on the projector screen (1) and the position of the finger at the phone screen is the position of the mouse pointer at the teaching material unit. According to the invention, on the basis of combination of the smart phone and the teaching, a loudspeaker and a pointing tool are unified and are installed at the smart phone. The equipment are simple and can be found easily; the operation is convenient and easy popularization can be realized, so that some defects in the existing multi-media teaching approach can be overcome. Moreover, software only needs to be installed by one time and can be used repeatedly by multiple times; the phenomenon that the teacher holds a laser pen in one hand and a loudspeaker in the other during teaching can be avoided, so that the teaching becomes convenient; and the learning efficiencies of students in the classroom can be improved beneficially and the multi-media teaching approach development can be promoted.
Owner:NANJING DAWU EDUCATION TECH

Amphiphilic C-6-(4-(methyl amino)-1,2,3-triazole)deoxidized inulin derivatives and preparation and application thereof

ActiveCN103694377AImprove high-value utilizationHigh reactivityAntibacterial agentsBiocideInulinLithium azide
The invention relates to amphiphilic C-6-(4-(methyl amino)-1,2,3-triazole)deoxidized inulin derivatives and a preparation and an application thereof. The amphiphilic C-6-(4-(methyl amino)-1,2,3-triazole)deoxidized inulin derivatives are as shown in formula (1), wherein n has an average range of 10-35. The preparation method comprises the following steps: halogenating the primary hydroxyl group of raw material inulin, performing acyl protection of hydroxy groups at the other sites, allowing the inulin to react with sodium azide or lithium azide at 40-70 DEG C for 8-24 hours, performing purification to obtain 6-azido-3,4-diacyl-6-deoxidized inulin, allowing the 6-azido-3,4-diacyl-6-deoxidized inulin to react with propynylamine through a click chemistry reaction to obtain the amphiphilic C-6-(4-(methyl amino)-1,2,3-triazole)deoxidized inulin derivatives. The mole amount of the sodium azide or lithium azide is 1-2 times as many as the that of the raw material inulin; the mole ratio of the propynylamine to the raw material inulin is 2-3:1. The product of the invention is wide in application, simple in synthetic steps, easy to popularize, and easily available in required equipment and raw materials.
Owner:YANTAI INST OF COASTAL ZONE RES CHINESE ACAD OF SCI

Rose rice wine oral liquid

The invention belongs to the technical field of healthcare product processing and relates to a rose rice wine oral liquid. Rose petals are used as main raw materials, Jimo rice wine, okra, Chinese wolfberries, dried figs, hawthorn fruits and honey are added, and the rose rice wine oral liquid with healthcare and conditioning functions is prepared. Firstly, the hawthorn fruits and the okra are cut into slices, placed into a stainless steel container and soaked in purified water, then the Chinese wolfberries and the dried figs are added, the mixture is heated and filtered, a mixed liquid is obtained for use, then fresh rose petals are collected, rinsed and placed in the container, after the mixed liquid is added, the mixture is heated and pulped, rose petal pulp is prepared, left to stand, cooled and filtered, a mixed rose liquid is obtained, finally, the Jimo rice wine is added to the rose mixed liquid, the mixture is stirred, heated, subjected to high-temperature sterilization and cooled to the room temperature, the honey is added, the mixture is evenly stirred, and a finished rose rice wine oral liquid product is obtained. The technology is mature, equipment is easy to obtain, and the product has high healthcare and nutritional value, and is convenient to eat, economical, practical, sanitary, safe and friendly in production and eating environment.
Owner:于希萌

Chitose aquagel evoked original position synthesis of super-paramagnetism nano ferriferrous oxide particles

The invention provides superparamagnetic nano Fe3O4 particles synthesized through in-situ induction of chitosan hydrogels, relating to a method for synthesizing the superparamagnetic nano Fe3O4 particles. The invention solves the problems of serious aggregation of the nano Fe3O4 particles and the complicated method for inducing the chitosan into the surface of the Fe3O4 in the current nano Fe3O4 particles. The method of the invention is that: 1. the chitosan powder is added into dilute acid solution; 2. cross-linking agent is added to make the chitosan hydrogels; 3. the chitosan hydrogels aresequentially dipped in Fe3+ aqueous solution, water, Fe2+ aqueous solution and water, and a plurality of times of circular leaching are made so as to form the chitosan hydrogels that contains iron ions; 4. then basification treatment is carried out; 5. the hydrogels is dissolved or degraded again, and finally the black superparamagnetic Fe3O4 nano particles are obtained upon centrifugalization. The method of the invention requires simple technique and mild conditions and the equipment used in the method is simple and can be obtained easily, thereby mass production can be achieved. The averagediameter of the particles is 15 to 25nm, and the particles distribute evenly with superparamagnetism.
Owner:HARBIN INST OF TECH
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