Aloe extractive as methanal trapping agent and preparation method thereof
A formaldehyde trapping agent and technology of aloe extract, which is applied in the field of aloe extract and its preparation, can solve the problems of irritating odor, high volatility, unsuitable for large-scale use, etc.
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Embodiment 1
[0024] Example 1: An aloe extract as a formaldehyde trap, prepared by using aloe as a raw material, and the preparation process includes the following steps:
[0025] Step 1: Hydrolyze the aloe gel: squeeze the aloe gel into juice, adjust the pH to 2.0 with 6mol / L hydrochloric acid, react at 100℃ for 5h, neutralize the hydrolysate with 20% NaOH by mass fraction, and then A small amount of impurities are removed from the centrifuge to obtain aloe gel hydrolysate. This step can hydrolyze the aloe vera gel and expose more amino groups.
[0026] Step 2: Under the protection of nitrogen, the above-mentioned aloe gel hydrolysate is added with the initiator cerium ammonium nitrate and acrylamide respectively. The mass ratio of the aloe gel hydrolyzate and the initiator cerium nitrate is 1:0.1 (with aloe gel Hydrolyzed liquid based on dry basis), the molar ratio of hydroxyl and acrylamide in the aloe gel hydrolyzed liquid is 1:6, and the three are evenly mixed and reacted at 50°C for 4 ho...
Embodiment 2
[0028] Example 2: An aloe extract as a formaldehyde trap, prepared by using aloe as a raw material, and the preparation process sequentially includes the following steps:
[0029] Step 1: Hydrolyze the aloe vera gel: squeeze the aloe vera gel into juice, adjust the pH to 8.5 with 20% NaOH, add 0.2% alkaline protease (based on the mass of the protein in the aloe vera gel), and heat up to 50 After 3 hours of reaction, the temperature is raised to 100°C to inactivate the enzyme, and the impurities in the product are removed in a centrifuge to obtain aloe gel hydrolysate;
[0030] Step 2: Under the protection of nitrogen, the above-mentioned aloe gel hydrolysate is added with initiator cerium ammonium nitrate and acrylamide respectively, and the mass ratio of the aloe gel hydrolyzate and initiator cerium ammonium nitrate is 1:0.4 (with aloe gel Hydrolyzed liquid based on dry basis), the molar ratio of hydroxyl and acrylamide in the aloe gel hydrolyzed liquid is 1:4, and the three are m...
Embodiment 3
[0032] Example 3: An aloe extract as a formaldehyde trap, prepared by using aloe as a raw material, and the preparation process includes the following steps:
[0033] Step 1: Hydrolyze the aloe vera gel: squeeze the aloe vera gel into juice, adjust the pH to 3.5 with 3mol / L hydrochloric acid, add 1% acid protease (based on the mass of the protein in the aloe vera gel), and heat up to 45 After 5 hours of reaction, the temperature is raised to 100°C to inactivate the enzyme, and a small amount of impurities are removed in the centrifuge to obtain the aloe gel hydrolysate;
[0034] Step 2: Under the protection of nitrogen, the above-mentioned aloe gel hydrolysate is added with the initiator potassium permanganate and acrylamide, and the mass ratio of the aloe gel hydrolyzate and the initiator potassium permanganate is 1:0.2 (based on aloe Gel hydrolysate based on dry basis), the molar ratio of hydroxyl and acrylamide in the aloe gel hydrolysate is 1:5, and the three are mixed uniforml...
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