Method for forming rare earth film on metal surface and applications thereof
A metal surface, rare earth technology, applied in the field of forming rare earth film on metal surface, can solve the problems of limited use of chromate, difficult to meet the requirements of corrosion resistance, toxicity of hexavalent chromium, etc. effect of corrosion
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Embodiment 1
[0038] Example 1 AA5083 aluminum alloy is subjected to surface electric pulse deposition to form a Ce oxide film
[0039]Firstly, the AA5083 aluminum alloy is pretreated according to the above steps, that is, the surface of the AA5083 aluminum alloy is mechanically polished, cleaned, degreased, derusted, etc., and then the pretreated AA5083 aluminum alloy is placed in a 0.1mol / L Ce(NO 3 ) 3 In an ethanol solution, at a temperature of 25°C, with a stainless steel electrode as an anode, under a pulse voltage with an applied potential of 12V and a duty cycle of 50%, the duration of each pulse is 0.1 seconds, and the electric pulse deposition treatment time is 120 seconds. A uniform and dense rare earth cerium organic complex thin film was obtained by electric pulse deposition on the sample. Then, spray gas fireworks with a flame spray gun, burn the surface of the rare earth cerium organic complex film deposited on the surface of the aluminum alloy with a gas flame spray gun, an...
Embodiment 2
[0040] Example 2 AA6061 aluminum alloy is subjected to surface electric pulse deposition to form a Ce oxide film
[0041] The AA6061 aluminum alloy is first pretreated according to the above steps, that is, the surface of the AA6061 aluminum alloy is mechanically polished, cleaned, degreased, and rusted, and then the pretreated AA6061 aluminum alloy is placed in a 0.05mol / L Ce(NO 3 ) 3 In an ethanol solution, at a temperature of 30°C, with a graphite electrode as an anode, under a pulse voltage with an applied potential of 10V and a duty cycle of 60%, the duration of each pulse is 0.2 seconds, and the electric pulse deposition treatment time is 180 seconds. A uniform and dense rare earth cerium organic complex thin film was obtained by electric pulse deposition on the sample. Then, spray gas fireworks with a flame spray gun, burn the surface of the rare earth cerium organic complex film deposited on the surface of the aluminum alloy with a gas flame spray gun, and use the ou...
Embodiment 3
[0042] Example 3 AA5083 aluminum alloy is subjected to surface electric pulse deposition to form a Ce oxide film
[0043] Firstly, the AA5083 aluminum alloy is pretreated according to the above steps, that is, the surface of the AA5083 aluminum alloy is mechanically polished, cleaned, degreased, derusted, etc., and then the pretreated AA5083 aluminum alloy is placed in a 0.1mol / L Ce(NO 3 ) 3 In ethanol solution, at a temperature of 20°C, with a stainless steel electrode as an anode, under a pulse voltage with an applied potential of 12V and a duty cycle of 50%, the duration of each pulse is 0.1 seconds, and the treatment time of electric pulse deposition is 120 seconds. A uniform and dense rare earth cerium organic complex thin film was obtained by electric pulse deposition on the sample. Then, place the AA5083 aluminum alloy forming rare earth cerium organic complex film in the furnace tube of the carbon-fixing furnace, pass high-purity nitrogen (99.999%) for 30 minutes to ...
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