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Spinosad soluble agent and preparation method thereof

A spinosad and soluble technology is applied in the field of preparation of soluble spinosad containing botanical pesticide spinosad and spinosad soluble solution, which can solve the problems of low solubility and difficulty in popularization and use, and achieve The preparation process is simple, the scope of use is expanded, and the production conditions are mild

Inactive Publication Date: 2010-11-24
HEBEI YIHAI ANGENUO AGROCHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, since spinosad is insoluble in water and has very low solubility in organic solvents, the current spinosad pesticides mainly use suspension concentrates, emulsifiable concentrates, anticide baits, water emulsions and other dosage forms, because they cannot be prepared into solutions. , so it is more difficult to promote and use, and it has not been widely accepted by people.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A solutionable solution of spinosad, comprising spinosad technical product, emulsifier 0201B, methanol, ethylene glycol and water, wherein the mass fraction of each component is 2.95% of spinosad technical product, emulsifier 0201B 10.5%, methanol 15.8%, ethylene glycol 5.26%, water 65.5%.

[0019] The method for preparing this spinosad soluble solution is: take the original drug of spinosad, surfactant, auxiliary agent and water in proportion, place it in an enamel kettle, and fully Stir until a clear liquid is obtained, i.e. a solution of spinosad. In addition, in order to promote the dissolution of spinosad, ultrasound can also be used in the preparation process to induce dissolution.

Embodiment 2

[0021] A spinosad solution solution, comprising spinosad technical product, emulsifier 0201B, ethanol, ethylene glycol and water, wherein the mass fraction of each component is 6.22% of spinosad technical product, emulsifier 0201B 11.1%, ethanol 16.7%, ethylene glycol 5.56%, water 60.4%.

[0022] The preparation method of this spinosad solution is the same as in Example 1.

Embodiment 3

[0024] A spinosad solution solution, comprising spinosad technical, emulsifier 0203B, isopropanol, ethylene glycol, urea and water, wherein the mass fraction of each component is spinosad technical 27.8 %, emulsifier 0203B 10%, isopropanol 15%, ethylene glycol 5%, urea 5%, water 37.2%.

[0025] The preparation method of this spinosad solution is the same as in Example 1.

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PUM

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Abstract

The invention discloses a spinosad soluble agent which comprises the following components based on the mass fraction: 2.5%-28% of spinosad bulk drug, 10%-12% of surfactant, 21%-25% of adjuvant and 37%-66% of water. The invention further discloses a preparation method of the spinosad soluble agent, comprising the following steps: proportionally weighing the spinosad bulk drug, the surfactant, the adjuvant and water; placing the materials into a reaction bottle; and under the water bath condition at the temperature of 20-100 DEG C, fully stirring the materials into a transparent liquid to finally obtain the spinosad soluble agent. In the invention, the botanical pesticide spinosad can be dissolved in a solvent to obtain the spinosad soluble agent by adopting a simple, safe and environmental-friendly process, which lays a foundation for application and popularization of the spinosad soluble agent in agricultural production.

Description

technical field [0001] The invention relates to a chemical pesticide, in particular to a soluble formulation containing the botanical pesticide spinosad; the invention also relates to a preparation method of the spinosad soluble formulation. Background technique [0002] At present, the development of green pesticides, especially biopesticides, has attracted more and more attention. Among them, spinosad, a botanical pesticide, has attracted special attention because of its high activity, broad insecticidal spectrum, and environmental friendliness. However, since spinosad is insoluble in water and has very low solubility in organic solvents, the current spinosad pesticides mainly use suspension concentrates, emulsifiable concentrates, anticide baits, water emulsions and other dosage forms, because they cannot be prepared into solutions. , so it is more difficult to promote and use, and it has not been widely accepted by people. Therefore, the research and preparation of the...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N43/22A01N25/02A01P7/04
Inventor 郭武棣郭鹏郭兴国刘万仁王巍
Owner HEBEI YIHAI ANGENUO AGROCHEM
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