Method for preparing polymer composite material with fluorescent property
A technology of composite materials and fluorescent properties, which is applied in the field of preparation of polymer composite materials, and can solve the problems of unreported polymer composite materials
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Embodiment 1
[0020] (1) Preparation of basic zinc carbonate - solution reaction precipitation - hydrothermal treatment method:
[0021] Add 52.40 parts of ammonium carbonate aqueous solution with a concentration of 0.5 mol / L to 57.44 parts of zinc nitrate aqueous solution with a concentration of 0.5 mol / L, suction filter the resulting precipitate and wash it with distilled water, add it to the autoclave, add 45 parts of distilled water, After heat preservation at 200°C for 20 hours, suction filtration, washing with distilled water, and drying to obtain basic zinc carbonate, the thermal weight loss curve is as follows: figure 1 It can be seen from the figure that basic zinc carbonate begins to decompose at about 270°C, which can be applied to higher processing temperatures.
[0022] (2) Preparation of a polymer composite material with fluorescent properties:
[0023] 100 parts of carboxylated hydrogenated nitrile rubber and 8 parts of basic zinc carbonate were blended on a two-roll mill, a...
Embodiment 2
[0025] (1) Preparation of basic zinc carbonate - solution reaction precipitation - hydrothermal treatment method:
[0026] Add 52.40 parts of ammonium carbonate aqueous solution with a concentration of 0.5 mol / L to 57.44 parts of zinc nitrate aqueous solution with a concentration of 0.5 mol / L, suction filter the resulting precipitate and wash it with distilled water, add it to the autoclave, add 45 parts of distilled water, After heat preservation at 200°C for 30 hours, suction filtration, washing with distilled water, and drying to obtain basic zinc carbonate, the thermal weight loss curve is as follows: figure 1 It can be seen from the figure that basic zinc carbonate begins to decompose at about 270°C, which can be applied to higher processing temperatures.
[0027] (2) Preparation of a polymer composite material with fluorescent properties:
[0028] 100 parts of carboxylated hydrogenated nitrile rubber and 8 parts of basic zinc carbonate were blended on a two-roll mill, a...
Embodiment 3
[0030] (1) Preparation of basic zinc carbonate - solution reaction precipitation - hydrothermal treatment method:
[0031] Add 52.40 parts of ammonium carbonate aqueous solution with a concentration of 0.5 mol / L to 57.44 parts of zinc nitrate aqueous solution with a concentration of 0.5 mol / L, suction filter the resulting precipitate and wash it with distilled water, add it to the autoclave, add 45 parts of distilled water, After heat preservation at 200°C for 40 hours, filter with suction, wash with distilled water, and dry to obtain basic zinc carbonate, which has a thermal weight loss curve such as figure 1 It can be seen from the figure that basic zinc carbonate begins to decompose at about 270°C, which can be applied to higher processing temperatures.
[0032] (2) Preparation of a polymer composite material with fluorescent properties:
[0033] 100 parts of carboxylated hydrogenated nitrile rubber and 8 parts of basic zinc carbonate were blended on a two-roll mill, and v...
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