Multi-stage depressed collector material and preparation and surface treatment method thereof
A technology for surface treatment and collector, which is applied in the field of satellite traveling wave tube multi-stage step-down collector material and its preparation and surface treatment, which can solve the problems of low strength and difficult to guarantee the insulation performance of collector.
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[0074] 1. Using W and Cu as raw materials, the average particle size of W and Cu powder after bleaching treatment is 5-8 μm, and the volume ratio of W and Cu powder is formulated according to 45:55;
[0075] 2. Isostatic pressing after dry ball milling, molding pressure 200MPa;
[0076] 3. Sintering temperature: 1150±50°C, heat preservation for 4 hours to obtain a sintered body with a density greater than 95%;
[0077] 4. After ultrasonically cleaning and drying the sintered body with acetone, soak it in the chromic acid solution for 20-50 seconds and take it out;
[0078] 5. Deacidification and dehydration treatment: Soak the sample treated with chromic acid solution in distilled water and boil for 5-8 minutes. Repeat wash 3 times. Then dehydrate with acetone and dry.
[0079] 6. Hydrogen treatment: 950±20°C, duration 15-40 minutes, hydrogen dew point not higher than -35°C.
[0080] After processing by the process of the method of the present invention, the surface morpho...
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