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Preparing method for molybdenum oxide - polyaniline composite nanowire and nanotube

A molybdenum oxide, polyaniline technology, applied in nanotechnology, nanotechnology, nanostructure manufacturing and other directions, can solve the problems of difficult preparation and preservation of ion exchange precursors, strict restrictions on synthesis conditions, and complicated operations, and achieve good application and industry. Chemical prospect, product quality and the effect of high yield and high production efficiency

Inactive Publication Date: 2012-08-01
FUDAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The above methods are all molybdenum oxide-polyaniline composite membranes, and the operation is cumbersome, the ion exchange precursor is difficult to prepare and store, and the synthesis conditions are harsh.

Method used

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  • Preparing method for molybdenum oxide - polyaniline composite nanowire and nanotube
  • Preparing method for molybdenum oxide - polyaniline composite nanowire and nanotube
  • Preparing method for molybdenum oxide - polyaniline composite nanowire and nanotube

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Experimental program
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Effect test

Embodiment 1

[0048] 1.24g (NH 4 ) 6 Mo 7 o 24 4H 2 Dissolve O in 20 mL of distilled water, inject 1.67 g of aniline, and then add 1.0 mol / L hydrochloric acid dropwise until white precipitate appears (pH 4~5). Transfer to an oil bath at 50°C, react for 6 hours, wash the obtained product with ethanol several times, filter it with suction, and dry it at 50°C. The product is called a precursor. Dissolve 0.355g of the precursor in 10mLPSS, add distilled water after centrifugation, adjust the pH of the system to 1.0 with 0.5mol / L hydrochloric acid, add 0.143g of ammonium persulfate, and react at room temperature for 12 hours to obtain molybdenum oxide-polyaniline composite nanowires A.

Embodiment 2

[0050]Carry out experiment with the method for embodiment 1, ammonium molybdate wherein is changed into sodium molybdate, makes nanowire product A 1 .

Embodiment 3

[0052] Carry out experiment with the method for embodiment 1, change the concentration of ammonium molybdate wherein into 0.01mol / L (calculate in molybdenum atom), make nanowire product A 2 .

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Abstract

The invention belongs to the nano-material technical field, and relates to a preparing method for molybdenum oxide - polyaniline composite nanowire and nanotube. Molybdena - aniline hybrid nano wire precursor is obtained by using molybdate as the source of molybdenum and interacting with aniline,,and the molybdenum oxide - polyaniline composite nanowire and nanotube are obtained by respectively adjusting system pH value under the initiation of oxidizing agent. The nanowire and the nanotube prepared by the method of the invention have the characteristics of a composite construction of nanometer scale, controllable physical and chemical features, large specific surface area, uniform one-dimensional morphology and controllable thickness and length. The prepared composite molybdenum oxide - polyaniline composite nanowire and nanotube have important application value in many fields such as designing of advanced catalyst, electrocatalysis, electrochemical super capacitor, electrode material, sensor, thermoelectric material, the synthesis and application of advanced optics, electrical material and magnetism material.

Description

technical field [0001] The invention belongs to the technical field of nanometer materials, and in particular relates to a method for preparing molybdenum oxide-polyaniline composite nanowires and nanotubes. Background technique [0002] Research on the compounding of inorganic materials and high molecular conductive polymers at the nanoscale has attracted increasing attention. Studies have shown that the compounding of the two can combine their excellent physical and chemical properties and improve each other, making the properties of the compound easier to control and adjust. The prior art discloses that polyaniline has good surface stability, thermal stability and conductivity, and it is widely used in electrochemical capacitors, batteries, sensors and corrosion inhibitors. Molybdenum oxide has unique electrochemical properties and electrocatalytic properties. Combining molybdenum oxide and polyaniline materials at the nanoscale through organic-inorganic compounding will...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L79/02C08K3/22C08G73/02B82B3/00
Inventor 唐颐王思浓高庆生张亚红
Owner FUDAN UNIV
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