Laser-marked and halogen-free flame-retardant polyamide composite material
A flame retardant polyamide and laser marking technology, which is applied in the field of halogen-free flame retardant polyamide composite materials and can be laser marked, can solve the problem of lack of clear laser marking ability, flame retardant performance that does not meet the requirements of use, and long-term durability. Can not meet and other problems, to achieve the effect of convenient laser marking, clear marking and high processing efficiency
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Embodiment 1
[0031] Embodiment 1: a laser-markable, halogen-free flame retardant polyamide composite material, comprising:
[0032] A) The amount of at least one polyamide resin is 25-80 parts, the preferred solution is about 45-75 parts or the sum of the amount of one or more polyamide resins, and the polyamide resin refers to nylon 6, nylon 66, or nylon 6 and nylon 66 blend; the melting temperature range of the polyamide resin is about 200~280℃, the more preferred melting temperature range is controlled at 220~270℃, and the relative viscosity range of the polyamide resin is preferably 2.15~280℃ 2.75.
[0033] B) At least one or several inorganic filler materials and the one or several inorganic filler materials and refers to one of glass fiber, talc, wollastonite, or a blend of two or three thereof.
[0034]C) At least one or more halogen-free flame retardants with flame retardant properties, and the one or more halogen-free flame retardants with flame retardant properties refer to phos...
Embodiment 1-1
[0037] Example 1-1: 50% by weight of nylon 66 (Pingdingshan Shenma: EPR27), 30% by weight of MPP (Melapur 200), 0.5% by weight of laser marking auxiliary (self-made), 0.25% by weight of N,N '-bis-(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionyl)hexamethylenediamine (provided by Zhongqing Chemical Industry Co., Ltd.), 0.25% by weight of tris[2.4-di-tert-butylphenyl] ] Phosphite (provided by Rianlong) and 0.3% by weight of pentaerythritol stearate were stirred in a high-speed mixer for 5 minutes, after mixing uniformly, put into a twin-screw extruder for extrusion and granulation, and add 20% by weight to the side feeder % short glass fiber (international composite alkali-free short glass fiber), the length-diameter ratio of the twin-screw extruder is 40:1, the screw speed is 265rpm / min, and the temperature of each zone of the screw is 260°C in the first zone and 260°C in the second zone. The second zone is 260°C, the third zone is 260°C, the fourth zone is 260°C, the fifth zone ...
Embodiment 1-2
[0038] Example 1-2: 35% by weight of nylon 66 (Pingdingshan Shenma: EPR27), 10% by weight of nylon 6 (1013B), 30% by weight of MPP (Melapur 200), 0.5% by weight of laser marking auxiliary ( Homemade), 0.25 wt% of N,N'-bis-(3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionyl)hexamethylenediamine, 0.25 wt% of tris[2.4-di-tert. Butylphenyl] phosphite and 0.5% by weight of pentaerythritol stearate were stirred in a high-speed mixer for 5 minutes. After mixing uniformly, they were put into a twin-screw extruder for extrusion and granulation, and 25% by weight of Short glass fiber (international composite alkali-free short glass fiber), the length-diameter ratio of the twin-screw extruder is 40:1, the screw speed is 265rpm / min, and the temperature of each zone of the screw is 260°C in the first zone and 260°C in the second zone. 260°C, the third zone 260°C, the fourth zone 260°C, the fifth zone 255°C, the sixth zone 255°C, the seventh zone 255°C, the eighth zone 255°C, the ninth zone 255...
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