Novel gas diffusion layer used for fuel cell, preparation and application
A gas diffusion layer and fuel cell technology, which is applied in the parts of fuel cells, fuel cells, electrical components, etc., can solve problems such as shortages, improve mass transfer and electrical conductivity, high-efficiency drainage and gas-conducting functions, and realize drainage. and the effect of air conduction
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Embodiment 1
[0031] Using ammonium carbonate as a pore-forming agent, the gas diffusion layer was prepared in five layers by one-sided leveling process, and the electrode was prepared by CCS method.
[0032] 1. Preparation of Diffusion Layer
[0033] (1) Ingredients and first application
[0034] (a) According to the carbon paper area, press 0.8mg carbon powder / cm 2 For carbon paper, weigh XC-72 carbon powder and place it in a beaker, add absolute ethanol at the rate of 70ml ethanol / g carbon powder, ultrasonically oscillate, and stir for one minute.
[0035] (b) According to carbon powder weight: PTFE dry weight = 1: 1.5, weigh 30% (wt.) water-repellent PTFE emulsion. Add dropwise into the feed liquid, ultrasonically oscillate, and stir for 2 minutes until the feed liquid becomes ink-like.
[0036] (c) According to carbon powder weight: pore-forming agent dry weight = 1:1.9, weigh the ammonium carbonate pore-forming agent sieved through 400 mesh and add it to the above-mentioned feed li...
Embodiment 2
[0054] Using ammonium oxalate as a pore-forming agent, the gas diffusion layer was prepared in five layers by one-sided leveling process, and the electrode was prepared by CCM method.
[0055] The preparation of the diffusion layer is the same as that in Example 1. Ammonium oxalate is used instead of ammonium carbonate as a pore-forming agent when preparing the leveling material of the gas diffusion layer. The preparation of the catalytic layer adopts the CCS method, and catalysts are prepared on both sides of the proton exchange membrane according to the known methods in the literature. To form an electrode, two prepared gas diffusion layers are sandwiched between the two sides of the CCS method electrode to assemble an MEA. This MEA is numbered B# and placed in a fuel cell evaluation device for testing.
Embodiment 3
[0057] Using ammonium chloride as pore-forming agent, the gas diffusion layer was prepared in five layers by one-side leveling process, and the electrode was prepared by CCS method.
[0058] The preparation method of the diffusion layer and the catalytic layer is the same as in Example 1, except that the pore-forming agent is changed to ammonium chloride.
[0059] The prepared two CCS method electrodes are sandwiched between the two sides of the proton exchange membrane to assemble the MEA. This MEA is numbered C# and placed in the fuel cell evaluation device for testing.
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