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Preparation method of karanjin

A technology of water xanthin and distilled water, applied in the direction of organic chemistry, can solve the problem of low water xanthin, achieve short separation time, good impurity removal effect, and realize the effect of batch preparation

Inactive Publication Date: 2011-11-16
NANJING ZELANG AGRI DEV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method is only to get a low content of lutein

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] Crush the dried medicinal material of Shuiluo umbrella, take 1kg, add appropriate amount of distilled water and 5g of biological enzymes for natural enzymolysis, and obtain enzymatic hydrolysis raw materials, put the enzymatic hydrolysis raw materials into the extraction equipment, add 12kg of 85% ethanol solution as solvent, and carry out continuous countercurrent extraction , the extraction temperature is 60°C, the extraction time is 2h, the extract is obtained, the extract is concentrated until it has no alcohol smell, it is adsorbed by the AB-8 macroporous resin column, first eluted with distilled water until the next column is colorless, and then 4L 70% The ethanol solution was eluted, the eluate was collected, concentrated and evaporated to dryness to obtain the crude product of luteolin; it was dissolved in 85% ethanol to make a solution with a concentration of 50 mg / ml, and filtered through a 0.45 μm microfiltration membrane to obtain a preparative high liquid pha...

Embodiment 2

[0016] Grind the dried medicinal materials of Shuiluo umbrella, take 1kg, add appropriate amount of distilled water and 5g of biological enzymes for natural enzymolysis, and obtain enzymatic hydrolysis raw materials, put the enzymatic hydrolysis raw materials into the extraction equipment, add 18kg of 85% ethanol solution as solvent, and carry out continuous countercurrent extraction , the extraction temperature is 65°C, the extraction time is 1h, the extract is obtained, the extract is concentrated until it has no alcohol smell, it is adsorbed by the LSA-21 macroporous resin column, first eluted with distilled water until the next column is colorless, and then 7L 70% The ethanol solution was eluted, the eluate was collected, concentrated and evaporated to dryness to obtain the crude product of lutein; it was dissolved in 85% ethanol to make a solution with a concentration of 80 mg / ml, and filtered through a 0.45 μm microfiltration membrane to obtain a preparative high liquid ph...

Embodiment 3

[0018] Crush the dried medicinal material of Shuiluo umbrella, take 1kg, add appropriate amount of distilled water and 5g of biological enzymes for natural enzymolysis, and obtain enzymatic hydrolysis raw materials, put the enzymatic hydrolysis raw materials into the extraction equipment, add 15kg of 85% ethanol solution as solvent, and carry out continuous countercurrent Extraction, the extraction temperature is 55°C, the extraction time is 1.5h, the extract is obtained, the extract is concentrated until it has no alcohol smell, it is absorbed by a D-101 macroporous resin column, first eluted with distilled water until the next column is colorless, and then 5L Elute with 70% ethanol solution, collect the eluent, concentrate and evaporate to dryness to obtain the crude product of lutein; dissolve it in 85% ethanol, make a solution with a concentration of 100 mg / ml, filter through a 0.45 μm microfiltration membrane, and prepare high The liquid chromatography preparative column u...

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Abstract

The invention relates to a preparation method of karanjin. The preparation method comprises the following steps: crushing dried Fordia cauliflora herbs, adding an appropriate amount of distilled water and a bioenzyme for natural hydrolysis to obtain enzymolysis raw materials, carrying out continuous countercurrent extraction on the enzymolysis raw materials with an 85% ethanol solution used as the solvent, concentrating the extract until no alcohol odor exists, adding the concentrated extract to macroporous resin for adsorption, concentrating the eluate, and drying to obtain a crude karanjin product, and separating by a preparative high-performance liquid chromatograph to obtain karanjin. The preparation method provided by the invention has the advantages of stable process, short period, high product yield, good product quality and high product purity (more than 98%).

Description

Technical field: [0001] The invention relates to a method for extracting and preparing active ingredients from plants, in particular to a method for preparing aquacetin. Background technique: [0002] Water xanthin, also known as water xanthin. Needle crystal, soluble in methanol, ethanol, chloroform, benzene, ether, almost insoluble in petroleum ether, dilute inorganic acid. Phantanthin has anti-mycobacterium tuberculosis effect and can be used for the treatment of vitiligo. [0003] Shuiluosan is the dried root of leguminous plant dried bean curd, which has the functions of dispelling blood stasis, reducing swelling, relieving pain, calming the mind, and improving intelligence. Postpartum and postpartum weakness embolism. This product is very rich in resources, mainly produced in Guangxi and Guangdong. It mainly contains active ingredients such as flavonoids, among which the content of lutein is as high as 0.45%. [0004] The extraction method of lutein is seldom disc...

Claims

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Application Information

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IPC IPC(8): C07D493/04
Inventor 苏刘花
Owner NANJING ZELANG AGRI DEV
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