High-temperature energy storage phase-change material and preparation and application thereof
A technology of energy storage phase change and high temperature, applied in the field of aluminum alloy high temperature energy storage phase change materials, can solve the problem of high latent heat in preparation, achieve high energy storage density, good thermal cycle performance, and improve energy conversion efficiency.
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Embodiment 1
[0015] The aluminum powder with a mass percentage of 60% and a purity of 99.5%, a magnesium powder with a mass percentage of 35% and a purity of 99.5% and a tin powder with a mass percentage of 5% and a purity of 99.0% are uniformly mixed Then, the balls were placed in a high-energy planetary ball mill at 500 R / min at a weight ratio of 50:1, and after ball milling for 5 hours, samples were taken by wet method.
[0016] Put the ball-milled product into a high-temperature tube furnace, under the protection of argon atmosphere, heat up to 500°C at 10°C / min and then roast for 3h. After the product is naturally cooled to room temperature, it is ground into powder to obtain the product.
[0017] Netzsch Proteus STA449 thermal analyzer was used to investigate the melting enthalpy of the alloy product. The experimental conditions are: sample dosage is about 10mg, 50ml / min argon atmosphere, heating rate 20°C / min, experimental temperature range 40-600°C, and measuring the enthalpy of melting...
Embodiment 2
[0019] The aluminum powder with a mass percentage of 60% and a purity of 99.5%, a magnesium powder with a mass percentage of 30% and a purity of 99.5% and a tin powder with a mass percentage of 10% and a purity of 99.0% are uniformly mixed Then, the balls were placed in a high-energy planetary ball mill at 500 R / min at a weight ratio of 50:1, and after ball milling for 5 hours, samples were taken by wet method.
[0020] Put the ball-milled product into a high-temperature tube furnace, under the protection of argon atmosphere, heat up to 600°C at 10°C / min, and then calcinate for 7 hours. After the product is naturally cooled to room temperature, the product is ground into powder.
Embodiment 3
[0022] The aluminum powder with a mass percentage of 60% and a purity of 99.5%, a magnesium powder with a mass percentage of 25% and a purity of 99.5% and a tin powder with a mass percentage of 15% and a purity of 99.0% are uniformly mixed Then, the balls were placed in a high-energy planetary ball mill at 500 R / min at a weight ratio of 50:1, and after ball milling for 5 hours, samples were taken by wet method.
[0023] Put the ball-milled product into a high-temperature tube furnace, under the protection of argon atmosphere, heat up at 10°C / min to 700°C and then roast for 5h. After the product is naturally cooled to room temperature, the product is ground into powder.
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