Method for preparing hydrogen fluoride and coproducing white carbon black with silicon tetrafluoride
A silicon tetrafluoride, hydrogen fluoride technology, applied in the direction of fluorine/hydrogen fluoride, silicon oxide, silicon dioxide, etc., can solve the problems of poor production safety, difficult filtration, incomplete conversion, etc., achieve huge environmental and social benefits, promote The effect of healthy and sustainable development and superior product quality
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Example Embodiment
[0021] Example 1
[0022] 700kg of crude silicon tetrafluoride gas produced by phosphate fertilizer is passed through a 300-mesh bag filter to remove sodium fluoride dust in the gas, and then passed through a two-stage activated carbon absorption column and a first-stage absorption column filled with 100-300℃ vacuum conditions The activated carbon is activated for 4 hours, and the secondary absorption column is filled with the activated carbon for 4 hours under the vacuum condition of 300-700℃. The activated carbon obtained by this method has higher activity and the lowest adsorption water content ( 2 , O 2 , H 2 , CO and CH 4 After the liquefied silicon tetrafluoride is gasified, it enters the next process of reaction. At this time, 684kg of silicon tetrafluoride gas with a purity of 99.99% is obtained.
[0023] Pass the purified 684kg silicon tetrafluoride gas and 245kg steam into the hydrolysis reactor at a rate of 1:2, and carry out the hydrolysis reaction at 300°C; the 530kg ...
Example Embodiment
[0024] Example 2
[0025] Purify 1000 kg of crude silicon tetrafluoride gas produced by phosphate fertilizer. The purification method is the same as the silicon tetrafluoride purification method in Example 1. The corresponding control conditions can be arbitrarily selected within its range to obtain tetrafluoride with a purity of 99.99%. 978kg of silicon fluoride gas. Then 978kg of silicon tetrafluoride gas and 337kg of water vapor are fed into the hydrolysis reactor at a rate of 1:2, and the hydrolysis reaction is carried out at 500°C; the 750kg of crude hydrogen fluoride gas produced by the hydrolysis is first introduced into the dust collector to remove dust and other solid impurities. The dust collector adopts a plate type dust collector and a bag type dust collector. The hydrogen fluoride gas after dust removal enters the first-stage rectification tower, and the condensation temperature at the top of the tower is controlled at 50 ℃, so that the hydrogen fluoride is condense...
Example Embodiment
[0026] Example 3
[0027] Purify 800 kg of crude silicon tetrafluoride gas by-product of phosphate fertilizer. The purification method is the same as the purification method of silicon tetrafluoride in Example 1. The corresponding control conditions can be arbitrarily selected within the range to obtain tetrafluoride with a purity of 99.99%. 785kg of silicon fluoride gas. Then 785kg of silicon tetrafluoride gas and 270kg of water vapor are introduced into the hydrolysis reactor at a rate of 1:2, and the hydrolysis reaction is carried out at 200°C; the 600kg of crude hydrogen fluoride gas produced by the hydrolysis is first introduced into the dust collector to remove dust and other solid impurities. The dust collector adopts a plate type dust collector and a bag type dust collector. The hydrogen fluoride gas after dust removal enters the first-stage rectification tower, and the condensation temperature at the top of the tower is controlled at 30 ℃, so that the hydrogen fluoride ...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap