Natural antibacterial textile containing fructus forsythiae extractive and preparation method thereof
A kind of forsythia extract, natural antibacterial technology, applied in the field of textiles, can solve the problems such as there is no literature record of forsythia extract, achieve obvious antibacterial effect, simple preparation process, and strong antibacterial activity
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Embodiment 1
[0019] Example 1 A preparation method of natural antibacterial textiles containing forsythia extract
[0020] (1) Preparation of microcapsules: Weigh 10 parts of forsythia extract, 1 part of polyvinyl alcohol, 30 parts of glutaraldehyde, and 2 parts of emulsifier, mix the forsythia extract and polyvinyl alcohol aqueous solution, mix well and inject The continuous phase of 1 part of emulsifier was emulsified in n-hexane at high speed at a speed of 700r / min to prepare emulsion A; mix glutaraldehyde with 5 drops of 10% hydrochloric acid aqueous solution, mix well and pour into another part of continuous phase containing 1 part of emulsifier High-speed emulsification in n-hexane at a speed of 700 to prepare emulsion B; mix the two emulsions A and B at 10°C, stir at high speed for 0.5h, filter, wash with petroleum ether three times, and freeze-dry at -10°C to obtain microcapsules;
[0021] (2) Use the printing method to fix the microcapsules on the base fabric:
[0022] Process ...
Embodiment 2
[0029] Embodiment 2 A kind of preparation method of the natural antibacterial textile containing forsythia extract
[0030] (1) Preparation of microcapsules: Weigh 30 parts of forsythia extract, 10 parts of polyvinyl alcohol, 60 parts of glutaraldehyde, and 30 parts of emulsifier, mix the forsythia extract and polyvinyl alcohol aqueous solution, mix well and inject The continuous phase of 15 parts of emulsifier is emulsified at high speed in n-hexane, and the rotation speed is 2500r / min, to prepare emulsion A; mix glutaraldehyde with 10 drops of 30% hydrochloric acid aqueous solution, mix well and inject another part of continuous phase containing 15 parts of emulsifier High-speed emulsification in n-hexane at a speed of 2500r / min to prepare emulsion B; mix the two emulsions A and B at 30°C, stir at high speed for 2 hours, filter, wash with petroleum ether for 5 times, and freeze-dry at -5°C to obtain microcapsules ;
[0031] (2) Use the printing method to fix the microcapsul...
Embodiment 3
[0039] Embodiment 3 A kind of preparation method of the natural antibacterial textile containing forsythia extract
[0040] (1) Preparation of microcapsules: Weigh 20 parts of forsythia extract, 5 parts of polyvinyl alcohol, 40 parts of glutaraldehyde, and 20 parts of emulsifier, mix the forsythia extract and polyvinyl alcohol aqueous solution, mix well and inject The continuous phase of 10 parts of emulsifier was emulsified in n-hexane at a high speed, and the rotation speed was 2000r / min to prepare emulsion A; mix glutaraldehyde with 7 drops of 20% hydrochloric acid aqueous solution, mix well and inject another part of continuous phase containing 10 parts of emulsifier High-speed emulsification in n-hexane at a speed of 2000r / min to prepare emulsion B; mix the two emulsions A and B at 20°C, stir at high speed for 1 hour, filter, wash with petroleum ether for 4 times, and freeze-dry at -8°C to obtain microcapsules ;
[0041] (2) Fix the microcapsules on the base cloth by pad...
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