Active packaging film based on essential oil/beta-cyclodextrin inclusion compound and preparation method for active packaging film
A technology of cyclodextrin inclusion compound and packaging film, which is applied in the field of packaging materials to achieve high-efficiency bacteriostatic activity, inhibited growth, and good transparency.
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[0027] Example 1
[0028] Take 40 g of polyvinyl alcohol, 1 g of sodium lauryl sulfate and 8 ml of ethylene glycol in a 500 ml beaker, and add 250 ml of water. Place the beaker in a constant temperature water bath and heat to 60° C. under low-speed stirring to obtain dispersion A. Weigh 5g of essential oil / β-cyclodextrin inclusion compound into a 250ml beaker, add 50ml water, and place the beaker in an ultrasonic oscillator for 15 minutes until the essential oil / β-cyclodextrin inclusion compound is more evenly dispersed in water. Get dispersion B. The dispersion liquid B is slowly added to the dispersion liquid A to form the dispersion liquid C. The dispersion liquid C is continuously heated to 95°C-100°C under low-speed stirring until the polyvinyl alcohol is completely melted. Take it out and cool to about 60°C and vacuum defoam to obtain a film-forming liquid. Put the film-forming liquid in a 50℃ water bath for heat preservation. Pour the film-forming liquid into the hopp...
Example Embodiment
[0029] Example 2
[0030] Take 40g of polyvinyl alcohol, 1g of sodium lauryl sulfate and 5ml of ethylene glycol in a 500ml beaker, and add 250ml of water. Place the beaker in a constant temperature water bath and heat to 60° C. under low-speed stirring to obtain dispersion D. Weigh 8g of essential oil / β-cyclodextrin inclusion compound into a 250ml beaker, add 50ml of water, and place the beaker in an ultrasonic oscillator for 15 minutes until the essential oil / β-cyclodextrin inclusion compound is more evenly dispersed in water. Get dispersion E. The dispersion liquid E is slowly added to the dispersion liquid D to be the dispersion liquid F. The dispersion liquid F is continuously heated to 95°C-100°C under low-speed stirring until the polyvinyl alcohol is completely melted. Take it out and cool to about 60°C and vacuum defoam to obtain a film-forming liquid. Put the film-forming liquid in a 50℃ water bath for heat preservation. Pour the film-forming liquid into the hopper o...
Example Embodiment
[0031] Example 3
[0032] Test results of active packaging film used for the preservation of sugar orange.
[0033] In this embodiment, sugar tangerine is used as a perishable food. Purchase seasonal sugar tangerines from the supermarket, and select the same size, no damage, no disease, ripe, fresh sugar tangerines. Wash the sugar tangerine with clean water first, then rinse with sterile water, and drain. The films prepared in Example 1 and Example 2 were cut into 15×15 cm squares and heat sealed into bags with a heat sealer. The fruits were randomly divided into multiple groups, and each group of 9 fruits was put into a film bag, and each treatment was repeated 3 times. The non-antibacterial PVA packaging film was used as a control to observe the effect of the active packaging film on the preservation of sugar tangerines. Thirty days after the start of the experiment, it was observed that the sugar tangerine in the packaging film prepared in the scheme of Example 2 did not rot...
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