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Method for sintering radially-oriented sintering samarium cobalt integrated magnetic ring

A sintering method and magnetic ring technology, which is applied in the direction of magnetic materials, magnetic objects, and inorganic materials, can solve problems such as large differences in product performance, easy cracking of magnetic rings, and narrow sintering uniform temperature zone, so as to improve the core competition in the market Strength, product temperature uniformity guarantee, and the effect of improving production yield

Active Publication Date: 2013-10-02
HUNAN AEROSPACE MAGNET & MAGNETO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This sintering method is adopted because the sintering uniform temperature zone of sintered samarium cobalt permanent magnet materials is narrow, and generally cannot exceed 5°C. If the temperature difference is large, it will lead to great differences in product performance, resulting in substandard magnetic properties of some products.
At present, this sintering method is roughly 5-30 kg per furnace. This sintering method not only consumes a lot of energy, but also has a small amount of sintering and low efficiency. Moreover, the vacuum tube repeats high and low temperature processes in a high temperature air environment, which is easy to oxidize. Thin and needs to be replaced often
It is understood that there are also very few internal heating vacuum furnaces, that is, the resistance heating device is arranged in the vacuum furnace. After the heating device heats up, the product is directly heated. The advantage of this sintering method is that the amount of firing is large, and the disadvantage is that the temperature uniformity is poor. , the temperature uniformity must be adjusted by some special means, which has not been reported in the literature
Using these two methods to sinter radially oriented monolithic magnetic rings has the problem that the magnetic rings are easy to crack, and the yield of products after sintering is extremely low, resulting in high production costs.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Take the radially oriented sintered samarium cobalt permanent magnet material overall magnetic ring blank φ45×φ31×12, and place them neatly in a heat-resistant stainless steel burning box (4 pieces per box), and put the 8 stacked together Put the box on the bracket, send it into the vacuum sintering furnace, cover the furnace door, and when the vacuum is lower than 0.05Pa, start the resistance heating device and the microwave heating device, heat up to 350 ° C, stop the microwave heating device, at 350 Keep warm for 30 minutes at ℃ to discharge the organic matter and adsorbed gas in the magnetic ring. At the end of the 350°C heat preservation, start the microwave heating device to continue heating. When the temperature rises to 850°C, stop the microwave heating device, and keep the temperature at 850°C for 30 minutes for pre-burning. At the end of the 850°C heat preservation, start the microwave heating device to continue heating. When the temperature rises to 1150°C, s...

Embodiment 2

[0021] Take the radially oriented sintered samarium-cobalt permanent magnet material overall magnetic ring blank φ45×φ31×12, and place them neatly in a heat-resistant stainless steel burning box (4 pieces per box), and put the 12 stacked pieces together Put the box on the bracket, send it into the vacuum sintering furnace, cover the furnace door, and when the vacuum is lower than 0.05Pa, start the resistance heating device and the microwave heating device, heat up to 350 ° C, stop the microwave heating device, at 350 Keep warm for 60 minutes at ℃ to discharge the organic matter and adsorbed gas in the magnetic ring. At the end of the heat preservation at 350°C, start the microwave heating device to continue heating. When the temperature rises to 850°C, stop the microwave heating device, keep the temperature at 850°C for 10 minutes, and carry out pre-burning. At the end of the heat preservation at 850°C, start the microwave heating device to continue heating. When the temperatu...

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PUM

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Abstract

The invention discloses a method for sintering a radially-oriented sintering samarium cobalt integrated magnetic ring and aims to solve the problems that in the conventional sintering method, the radially-oriented sintering samarium cobalt integrated magnetic ring is susceptible to cracking and has low finished product rate and the production cost is greatly increased. According to the method, the pressed radially-oriented sintering samarium cobalt integrated magnetic ring is placed into a novel vacuum sintering furnace, and heating and heat preservation are performed by the heating method of combining the traditional resistance heating with the microwave heating, so that the temperature of the magnetic ring is increased uniformly, thermal stress generated by that the magnetic ring is heated non-uniformly due to heating of a traditional resistance is reduced, the integrity of the magnetic ring is maintained, the finished product rate is increased, and the cost is reduced.

Description

technical field [0001] The invention relates to a sintering method of a sintered samarium cobalt permanent magnet material, in particular to a sintering method of a radially oriented sintered samarium cobalt integral magnetic ring. Background technique [0002] The sintering of existing sintered samarium cobalt permanent magnet materials is mostly carried out by external heating vacuum tube furnace (horizontal or vertical), and the resistance heating device is arranged outside the vacuum tube. Place the samarium cobalt product in the tube to make it reach the set temperature. This sintering method is adopted because the sintering uniform temperature zone of sintered samarium cobalt permanent magnet materials is narrow, and generally cannot exceed 5°C. If the temperature difference is large, it will lead to great differences in product performance, resulting in substandard magnetic properties of some products. . At present, this sintering method is roughly 5-30 kg per furn...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F3/16H01F1/055H01F1/08
Inventor 谭春林罗明李彬胡娟万绍平文晓林
Owner HUNAN AEROSPACE MAGNET & MAGNETO
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