Size mixture for sizing filament, and preparation method and application of size mixture

A technology of mixture and sizing, applied in textile and paper making, fiber type, fiber processing and other directions, can solve the problems of sizing adhesion, insufficient abrasion resistance, moisture absorption of sizing, and large required amount, etc., to achieve performance improvement, The effect of easy desizing and reduced sizing rate

Inactive Publication Date: 2012-09-12
苏州瀚海化学有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to provide a sizing mixture for filament sizing, which solves the problem of insufficient sizing adhesiveness and wear resistance in polyester filament sizing in the prior art, requires a large amount, and easily causes sizing to absorb moisture and Sticky and other problems

Method used

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  • Size mixture for sizing filament, and preparation method and application of size mixture
  • Size mixture for sizing filament, and preparation method and application of size mixture
  • Size mixture for sizing filament, and preparation method and application of size mixture

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] 1. Preparation of water-soluble polyester:

[0046] 95.8kg terephthalic acid, 12kg isophthalic acid, 15.6kg dimethyl isophthalate-5-sodium sulfonate, 8kg 1,4-cyclohexanedicarboxylic acid, 40.1kg ethylene glycol, 16.6kg new Put pentylene glycol and 50g of isopropyl titanate into the reaction kettle, replace the air with nitrogen to discharge the air, stir and raise the temperature, and react at 220-255°C. When the by-products reach the theoretical value, reduce the pressure and polymerize, the reaction temperature is 250-280 ° C, stop the reaction after reaching the end point, fill with nitrogen to eliminate the vacuum, and extrude the material.

[0047] 2. Synthesis of acrylic paste:

[0048] Mix the following monomers well:

[0049]

[0050]

[0051]First add the emulsifier sodium lauryl sulfate (2-4% of the total amount of monomers) and water (3.2 times the total amount of monomers) into the reaction kettle equipped with a reflux condenser, and stir evenly. T...

Embodiment 2

[0054] 1. Preparation of water-soluble polyester:

[0055] 105kg terephthalic acid, 23kg isophthalic acid, 13.2kg dimethyl isophthalate-5-sodium sulfonate, 5kg adipic acid, 53kg ethylene glycol, 23.4kg1,4-butanediol, 46g di Put butyltin oxide and zinc acetate into the reaction kettle, replace the air with nitrogen, heat up with stirring, and react at 220-255°C. When the by-products reach the theoretical value, reduce the pressure and polymerize, the reaction temperature is 250-280 ° C, stop the reaction after reaching the end point, fill with nitrogen to eliminate the vacuum, and extrude the material.

[0056] 2. Synthesis of acrylic paste:

[0057] Mix the following monomers well:

[0058]

[0059] First add the emulsifier sodium lauryl sulfate (2-4% of the total amount of monomers) and water (3.2 times the total amount of monomers) into the reaction kettle equipped with a reflux condenser, and stir evenly. Then add the previously mixed monomer and initiator (potassium ...

Embodiment 3

[0062] 1. Preparation of water-soluble polyester:

[0063] 95.8kg terephthalic acid, 12kg isophthalic acid, 15.6kg dimethyl isophthalate-5-sodium sulfonate, 8kg 1,4-cyclohexanedicarboxylic acid, 40.1kg ethylene glycol, 16.6kg new Put pentylene glycol and 50g of isopropyl titanate into the reaction kettle, replace the air with nitrogen to discharge the air, stir and raise the temperature, and react at 220-255°C. When the by-products reach the theoretical value, reduce the pressure and polymerize, the reaction temperature is 250-280 ° C, stop the reaction after reaching the end point, fill with nitrogen to eliminate the vacuum, and extrude the material.

[0064] 2. Synthesis of acrylic paste:

[0065] Mix the following monomers well:

[0066]

[0067] First add the emulsifier sodium lauryl sulfate (2-4% of the total amount of monomers) and water (3.2 times the total amount of monomers) into the reaction kettle equipped with a reflux condenser, and stir evenly. Then add the...

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PUM

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Abstract

The invention discloses a size mixture for sizing filament. The size mixture is characterized by comprising the following components in percentage by weight: 5 to 25 percent of water soluble polyester, and 75 to 95 percent of acrylic size, wherein the viscosity of the water soluble polyester is 0.35 to 0.6. The composite can be adhered to terylene well; the adhesion and the tensile property of the size are greatly improved; the permeability of the acrylic size can be improved, and the viscosity is reduced; and by matching the water soluble polyester and the acrylic size, the performance of the size can be improved. The sizing percentage is reduced, and cost is saved.

Description

technical field [0001] The invention belongs to the technical field of textile sizing, and in particular relates to a size mixture for filament sizing, a preparation method and application. Background technique [0002] Slurries are divided into two categories: natural and synthetic. The former includes starch, modified starch, alginate, etc. The latter uses carboxymethyl cellulose (CMC), polyvinyl alcohol, polyacrylate and the like. The two can also be mixed with each other. At present, the size of the domestic filament sizing is mainly acrylic size, but the film strength of the general acrylic size is not enough, and it is prone to slack. Moreover, in terms of polyester filament sizing, its adhesion and wear resistance need to be improved. In addition, if the amount is too large, the sizing will easily cause moisture absorption and stickiness. The present invention thus comes. Contents of the invention [0003] The purpose of the present invention is to provide a si...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/31D06M15/507C08G63/688C08F220/56C08F220/06C08F220/14C08F220/48D06M101/32
Inventor 金旭许峰叶同奇黄志远付静
Owner 苏州瀚海化学有限公司
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