Method for preparing grapheme platinum nanocomposite material by using argon plasma
A technology of composite materials and plasma, which is applied in the field of preparing graphene-platinum nanocomposites by ions, can solve the problems of complicated process, time-consuming and energy-consuming, and the introduction of impurities, and achieve simplified process, shortened preparation time, and good electrocatalytic performance Effect
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[0026] A method for preparing graphene-platinum nanocomposites with argon plasma, comprising the following steps:
[0027] A. Put 50mg of graphene oxide into a beaker, then add 2ml of 1 mol.L -1 The chloroplatinic acid, the mixture of gained is placed in oven and dried at 60 DEG C to obtain the powder of drying;
[0028] B. Place the dried powder in an airtight container (see figure 1 ), the container is connected with a graphite electrode, and the electrode is connected to an AC power supply, which can generate an inductively coupled plasma source, and then first pass argon gas into the container to drive away the air, and then turn on the vacuum pump to evacuate to 3Pa, and then turn on the AC The power supply generates argon plasma, and the plasma flow is directly applied to the surface of the dried powder for 30 minutes. After the discharge is completed, the reaction product is fully washed with deionized water or an appropriate organic solvent, filtered, and dried at 60°...
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