High mechanical strength ammonia storage mixture containing ceramic fiber and preparation method thereof
A technology of ceramic fiber and mechanical strength, which is applied in the field of hydrogen fuel cell system of new energy vehicles, can solve the problems that there are no clear claims and detailed items, and technical personnel cannot implement it, so as to achieve good physical adsorption and surface chemical activity, improve viscosity and Adsorption capacity, effect of structural stability
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Embodiment 1
[0015] The industrial anhydrous magnesium chloride salt powder of 69wt%, the ceramic fiber of 7wt%, the industrial clay of 7wt% and the industrial alcohol of 17wt% form a mixture, stir evenly by the mixer, stirring time is 1h, forms semi-dry mixed powder; The semi-dry mixed powder is added into an openable airtight container and subjected to mechanical vibration for 30 minutes to form a wet body sample, and then at 80°C with a vacuum of 10 -1 After drying for 2 hours under the condition of Kpa, an ammonia storage active mixture containing 8.4wt% ceramic fibers can be obtained.
[0016] Fill 10g of ammonia storage active mixture with ammonia in a naturally ventilated environment. Put the openable airtight container into a water tank with enough cooling water in advance, connect the ammonia steel cylinder, and pass through the pressure reducing valve and drying system , fill ammonia slowly within the pressure range of 1Mpa, and the ammonia filling time is 3h; after ammonia filli...
Embodiment 2
[0018] The industrial anhydrous magnesium chloride salt powder of 80wt%, the ceramic fiber of 4wt%, the industrial clay of 4wt% and the industrial alcohol of 12wt% form a mixture, stir evenly by the mixer, and stirring time is 5h, forms semi-dry mixed powder; The semi-dry mixed powder is added into an openable airtight container and mechanically shaken for 60 minutes to form a wet body sample, and then dried at 60°C for 3 hours under a vacuum of 1Kpa to obtain 4.5wt % Ammonia storage active mixture of ceramic fibers 。
[0019] Fill 10g of ammonia storage active mixture with ammonia in a naturally ventilated environment. Put the openable airtight container into a water tank with enough cooling water in advance, connect the ammonia steel cylinder, and pass through the pressure reducing valve and drying system , fill ammonia slowly within the pressure range of 0.3Mpa, and the ammonia filling time is 5h; after ammonia filling, the mass of the sample block is 19.9g, that is, 9.9g ...
Embodiment 3
[0021] The industrial anhydrous magnesium chloride salt powder of 75wt%, the ceramic fiber of 10wt%, the industrial clay of 4wt% and the industrial alcohol of 11wt% form a mixture, stir evenly by the mixer, stirring time is 10h, forms semi-dry mixed powder; The semi-dry mixed powder is added into an openable airtight container and subjected to mechanical vibration for 45 minutes to form a wet body sample, and then dried at 100°C for 3 hours to obtain a storage material containing 11.2wt% ceramic fibers. Ammonia Active Mixture 。
[0022] Fill 10g of ammonia storage active mixture with ammonia in a naturally ventilated environment. Put the openable airtight container into a water tank with enough cooling water in advance, connect the ammonia steel cylinder, and pass through the pressure reducing valve and drying system , fill ammonia slowly within the pressure range of 0.2Mpa, and the ammonia filling time is 8h; after ammonia filling, the mass of the sample block is 19.1g, that...
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