Method for transferring graphene film with static protective film as medium

A graphene film and protective film technology, applied in chemical instruments and methods, electronic equipment, lamination devices, etc., can solve the problems of comparison, transfer integrity and reliability, etc., and achieve convenient use, cost saving, and easy operation simple effect

Active Publication Date: 2012-11-14
WUXI GRAPHENE FILM +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method is only suitable for small-area transfer, and its transfer integrity and reliability cannot be compared with the "corrosion matrix method" with a medium, so this method has great limitations in application

Method used

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  • Method for transferring graphene film with static protective film as medium
  • Method for transferring graphene film with static protective film as medium

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] A method for transferring multilayer graphene using electrostatic protection film, comprising the following steps:

[0064] (1) Use copper foil as a substrate to prepare graphene film by vapor phase deposition method, sandwich the copper foil with graphene between two pieces of glass, and apply a certain force to make the surface of the copper foil film flat and less wrinkled; The film machine completely laminates the PP electrostatic protective film and the copper foil with graphene, the lamination speed is 10mm / min, and the lamination temperature is room temperature;

[0065] (2) Put the electrostatic protective film / copper foil with graphene combination into the ammonium persulfate solution to etch, with the side of the electrostatic protective film facing up and the side of the copper foil facing down; after 10 minutes, remove the Clean the surface of the copper foil with ionized water and ethanol, and use the same method to clean twice in a row; etch for 3 hours, a...

Embodiment 2

[0071] A method for transferring multilayer graphene using electrostatic protection film, comprising the following steps:

[0072] (1) The graphene film with copper foil as the substrate is prepared by vapor deposition method, and the copper foil with graphene is rolled through the laminating machine to make the copper foil film very flat, and the laminating speed is 200mm / min; Technology, the PET electrostatic protective film is attached to the copper foil with graphene; the lamination speed is 200mm / min, and the lamination temperature is room temperature;

[0073] (2) Put the combination of electrostatic protective film and copper foil with graphene into ferric chloride solution to etch. After 10 minutes, clean the surface of copper foil with deionized water and methanol. time; etch for 3h, and the copper foil is completely removed; then the graphene / static protective film is taken out from the ferric chloride solution, and the surface of the graphene / static protective film ...

Embodiment 3

[0079] A method for transferring multilayer graphene using electrostatic protection film, comprising the following steps:

[0080] (1) The graphene film with nickel foil as the substrate is prepared by vapor deposition method, and the copper foil with graphene is rolled through the laminating machine to make the nickel foil film very flat, and the laminating speed is 1000mm / min; Technology, attaching PVC electrostatic protective film to nickel foil with graphene; among them, the laminating speed is 1000mm / min;

[0081] (2) Etch the combination of electrostatic protective film and nickel foil with graphene in ferric nitrate solution; after 10 minutes, clean the surface of nickel foil with deionized water and methanol. times; etch for 3h, and the nickel foil is completely removed; then the graphene / static protective film is taken out from the ferric chloride solution, the surface of the graphene / static protective film is rinsed with deionized water and methanol, and dried at 60°...

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PUM

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Abstract

The invention relates to a method for transferring a graphene film with a static protective film as a medium. The method includes that the static protective film is attached to graphene containing a growing lining through an electrostatic adsorption effect, then the growing lining is removed, a graphene/static protective film combination is obtained, finally a single layer of the graphene/static protective film combination is attached to a target substrate, static is released, the static protective film is removed, and the single-layer graphene film is obtained; or after the single layer of the graphene/static protective film combination is obtained, the single-layer of the graphene/static protective film combination replaces the static protective film, attaching of the graphene/static protective film is conducted sequentially on the graphene containing the growing lining repeatedly, the growing lining is removed, and finally a plurality of layers of graphene films are obtained. The method is simple to operate and free of residual glue, and organic solvent for following washing is not required, and therefore process cost for transferring the graphene films is reduced.

Description

technical field [0001] The invention relates to a method for transferring a graphene film, in particular to a method for transferring a single-layer or multi-layer graphene film using an electrostatic protective film as a medium, and belongs to the field of conductive film materials. Background technique [0002] Graphene thin films have high light transmittance and extremely high carrier mobility, and have great application prospects in electronic devices and solar cells. In order to fabricate graphene electronic devices, the primary problem is to prepare large-scale graphene films and transfer them to suitable target substrates. [0003] The transfer technology of graphene film is a method of transferring graphene between different substrates, usually transferring graphene from a growth substrate to a target substrate. The transfer technology of graphene film is the key factor restricting the development of graphene film. The ideal transfer technology should have the foll...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B32B37/00B32B38/10
CPCB32B37/00B32B38/10C01B31/04B32B37/025B32B2313/04B32B2457/10
Inventor 邱玉锐谭化兵王振中
Owner WUXI GRAPHENE FILM
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