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Preparation method and preparation mold of amorphous alloy-copper laminated composite material

A technology of amorphous alloys and composite materials, applied in manufacturing tools, non-electric welding equipment, metal processing equipment, etc., can solve the problems of uneven longitudinal distribution of core materials, insufficient removal of oxide film at the connection interface, and large deformation. To achieve the effect of good interface integration, ensure accuracy, and tightly connect the interface

Active Publication Date: 2013-01-02
NORTHWESTERN POLYTECHNICAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] In order to overcome the deficiencies existing in the prior art or that the deformation of the sample is large, the removal of the oxide film at the connection interface is insufficient, the composite interface has obvious defects, or the core material is unevenly distributed in the longitudinal direction, the present invention proposes an amorphous Preparation method of alloy-copper layered composite material and preparation mold

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  • Preparation method and preparation mold of amorphous alloy-copper laminated composite material
  • Preparation method and preparation mold of amorphous alloy-copper laminated composite material
  • Preparation method and preparation mold of amorphous alloy-copper laminated composite material

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Embodiment 1

[0034] The present embodiment is a kind of preparation method of the layered composite material of amorphous alloy-copper, and described amorphous alloy is made of Zr 41.25 Ti 13.75 Cu 12.5 Ni 10 be22.5 A bar with a diameter of Φ5mm is produced; the copper is a T2 copper tube of Φ6mm×1mm. The concrete process of this embodiment is:

[0035] Step 1, surface treatment: Pass the amorphous alloy rod through the lathe to Φ4.2mm, and the outer surface of the amorphous alloy rod and the inner wall of the T2 copper tube are successively passed through 240#, 400#, 800#, 1000#, 1500#, 2000# sandpaper Sand until the surface is smooth without scratches. Use 5% hydrochloric acid alcohol treatment to remove the oxide film on the surface of the T2 copper tube. The surface-treated amorphous alloy rods and T2 copper tubes were ultrasonically cleaned with acetone by a conventional method and placed in a mold.

[0036] Step 2, vacuum pre-pressing: place the assembled mold in a vacuum diffu...

Embodiment 2

[0041] The present embodiment is a kind of preparation method of the layered composite material of amorphous alloy-copper, and described amorphous alloy is made of Zr 41.25 Ti 13.75 Cu 12.5 Ni 10 be 22.5 A bar with a diameter of Φ5mm is produced; the copper is a T2 copper tube of Φ6mm×1mm. The concrete process of this embodiment is:

[0042] Step 1, surface treatment: Pass the amorphous alloy rod through the lathe to Φ4.2mm, and the outer surface of the amorphous alloy rod and the inner wall of the T2 copper tube are successively passed through 240#, 400#, 800#, 1000#, 1500#, 2000# sandpaper Sand until the surface is smooth without scratches. Use 5% hydrochloric acid alcohol treatment to remove the oxide film on the surface of the T2 copper tube. The surface-treated amorphous alloy rods and T2 copper tubes were ultrasonically cleaned with acetone by a conventional method and placed in a mold.

[0043] Step 2, vacuum pre-pressing: place the assembled mold in a vacuum dif...

Embodiment 3

[0048] The present embodiment is a kind of preparation method of the layered composite material of amorphous alloy-copper, and described amorphous alloy is made of Zr 41.25 Ti 13.75 Cu 12.5 Ni 10 be 22.5 A bar with a diameter of Φ5mm is produced; the copper is a brass tube with a diameter of Φ6mm×1mm. The concrete process of this embodiment is:

[0049] Step 1, surface treatment: pass the amorphous alloy rod through the lathe to Φ4.2mm, the outer surface of the amorphous alloy rod and the inner wall of the brass tube are passed through 240#, 400#, 800#, 1000#, 1500#, 2000# sandpaper in sequence Sand until the surface is smooth without scratches. Use 5% hydrochloric acid alcohol treatment to remove the oxide film on the surface of the brass tube. The surface-treated amorphous alloy rods and brass tubes were ultrasonically cleaned with acetone by a conventional method and placed in a mold.

[0050] Step 2, vacuum pre-pressing: place the assembled mold in a vacuum diffusio...

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Abstract

The invention relates to a preparation method and preparation mold of an amorphous alloy-copper laminated composite material. The amorphous alloy is an amorphous alloy bar made of 41.25% of Zr, 13.75% of Ti, 12.5% of Cu, 10% of Ni and 22.5% of Be; and the copper is a red copper tube or a brass tube. The outer diameter of the bar is the same with the inner diameter of the copper tube. The preparation method comprises the following steps: under a room-temperature vacuum environment, removing oxide films on the surfaces of the amorphous alloy and the copper through the rubbing effect between the amorphous alloy and the copper; and then heating in vacuum to a temperature in the temperature range of a supercooled liquid region of the amorphous alloy, and keeping the temperature for a period of time to enable the amorphous alloy and the copper to be subjected to atomic diffusion, thus preparing the amorphous alloy-copper laminated composite material. The prepared amorphous alloy-copper laminated material has a tight connection interface between the amorphous alloy and the copper, and the interface is straight and level without any diffusion connection defect such as perforation and the like.

Description

technical field [0001] The invention belongs to the technical field of composite material preparation, and in particular provides a preparation method of an amorphous alloy-copper layered composite material and a special mold thereof. Background technique [0002] Due to its special atomic structure of long-range disorder and short-range order, amorphous alloys exhibit more excellent properties than traditional crystalline alloys, such as high strength, high hardness, high corrosion resistance, excellent magnetic properties and certain temperature Superplasticity within the range, etc., has shown great application value in the fields of aerospace devices, precision machinery and information. However, due to the poor room temperature plasticity and small critical size of amorphous alloys, the wide application of amorphous alloys is greatly restricted. Combining amorphous alloys and metals by diffusion bonding can give full play to the complementary advantages of the two on t...

Claims

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Application Information

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IPC IPC(8): B23K20/14B23K20/233B23K20/24B23K20/26
Inventor 李金山寇宏超王军胡锐常辉薛祥义钟宏张铁邦唐斌
Owner NORTHWESTERN POLYTECHNICAL UNIV
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