Laminated porous film, separator for non-aqueous electrolyte secondary battery, and non-aqueous electrolyte secondary battery
A non-aqueous electrolyte, secondary battery technology, used in secondary battery parts, battery pack parts, coatings, etc., can solve problems such as short circuit between two poles, separator membrane rupture, fire, etc. Excellent properties, the effect of excellent heat resistance
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Embodiment 1
[0244] Alumina (manufactured by Sumitomo Chemical Co., Ltd., Sumicorundum AA-03, average particle diameter: 0.3 μm) 39.4 parts by mass, polyvinyl alcohol (manufactured by Kuraray, PVA124, degree of saponification: 98.0 to 99.0, average degree of polymerization: 2400) 0.6 The mass parts were dispersed in 60.0 mass parts of water to obtain a dispersion liquid. Then, 0.003 parts by mass of polyethyleneimine (manufactured by Junsei Chemical Co., Ltd., polyethyleneimine 10000, molecular weight: about 10000) was dispersed in the dispersion liquid to obtain a dispersion liquid. At this time, the content rate of the adhesive agent (c) contained in a dispersion liquid was 0.05 mass % with respect to 100 mass % of resin binders (b).
[0245] The obtained dispersion liquid was coated on the laminated porous film obtained by the above-mentioned method for producing a polyolefin resin porous film with a gravure coater, and then dried at 60°C.
[0246] The physical properties of the obtain...
Embodiment 2
[0248] Alumina (manufactured by Sumitomo Chemical Co., Ltd., Sumicorundum AA-03, average particle diameter: 0.3 μm) 39.4 parts by mass, polyvinyl alcohol (manufactured by Kuraray, PVA124, degree of saponification: 98.0 to 99.0, average degree of polymerization: 2400) 0.6 The mass parts were dispersed in 60.0 mass parts of water to obtain a dispersion liquid. Then, 0.018 parts by mass of polyethyleneimine (manufactured by Junsei Chemical Co., Ltd., polyethyleneimine 10000, molecular weight: about 10000) was dispersed in the dispersion liquid to obtain a dispersion liquid. At this time, the content rate of the adhesive agent (c) contained in a dispersion liquid was 3 mass % with respect to 100 mass % of resin binders (b).
[0249] The obtained dispersion liquid was coated on the laminated porous film obtained by the above-mentioned method for producing a polyolefin resin porous film with a gravure coater, and then dried at 60°C.
[0250] The physical properties of the obtained ...
Embodiment 3
[0252]Alumina (manufactured by Sumitomo Chemical Co., Ltd., Sumicorundum AA-03, average particle diameter: 0.3 μm) 39.4 parts by mass, polyvinyl alcohol (manufactured by Kuraray, PVA124, degree of saponification: 98.0 to 99.0, average degree of polymerization: 2400) 0.6 The mass parts were dispersed in 60.0 mass parts of water to obtain a dispersion liquid. Then, 0.06 parts by mass of polyethyleneimine (manufactured by Junsei Chemical Co., Ltd., polyethyleneimine 10000, molecular weight: about 10000) was dispersed in the dispersion liquid to obtain a dispersion liquid. At this time, the content rate of the adhesive agent (c) contained in a dispersion liquid was 10 mass % with respect to 100 mass % of resin binders (b).
[0253] The obtained dispersion liquid was coated on the laminated porous film obtained by the above-mentioned method for producing a polyolefin resin porous film with a gravure coater, and then dried at 60°C.
[0254] The physical properties of the obtained l...
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