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Method for extracting active ingredient from maca

A technology of active ingredients and maca, applied in the field of extraction and purification of natural biological resources, can solve the problems of incomplete extraction of active ingredients of maca, unsuitable for large-scale production, poor stability of active ingredients, etc., so as to improve the comprehensive utilization value. , The effect of solving the material hardening and pipeline blockage and improving the extraction rate

Inactive Publication Date: 2013-01-30
JIANGSU JIANGDAYUAN ECOLOGICAL BIOLOGICAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the low extraction efficiency, cumbersome separation steps, poor stability of active ingredients and unsuitability for large-scale production in the traditional separation, extraction and purification technology of active ingredients in Maca, it has seriously affected the use of Maca in the fields of biomedicine and health care products. development and application of
[0004] Chinese patent literature discloses a kind of extracting method of Maca, and the patent title of this patent is " Maca active ingredient extracting method ", and the patent No. is " 01138330.5 ", and the step of this method is: after fresh Maca root is vacuum-dried, Pulverized into powder for later use, maca root powder is not used CO 2 + entrainer for supercritical CO 2 Extraction technology extraction, get the extract, add water and emulsifier to the extract, vacuum evaporate the concentrate, spray dry and granulate after homogeneous emulsification, this method uses supercritical carbon dioxide extraction, which can keep the active ingredients in the extract, and reduce the high boiling point, Substances with low volatility and easy pyrolysis are extracted at a temperature far below their boiling point, and there is no solvent residue in the extract, which prevents the existence of harmful substances to the human body and pollution to the environment during the extraction process, ensuring 100% Natural, but because Maca contains fat components and water-soluble components, this method can not completely extract the effective components of Maca

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Select fresh and high-quality maca rhizomes from Lijiang, Yunnan, and place them in a vacuum drying room at a vacuum degree of 0.08Mpa and a temperature of 45°C to vacuum dry to a moisture content of 6%; use liquid nitrogen low temperature pure physical wall breaking technology to break the wall After sieving treatment, the broken wall particle size is 100 mesh, and the dry maca powder is granulated by alcohol wet method, and the particle size is 14 mesh. Weigh 9 kg of maca granules and put them into the extraction container. C, CO 2 Extract at a flow rate of 20L / hr for 2 hours, then feed in 5% edible 95% ethanol as a carrier, and extract for another 1 hour. Through separation kettle 1 separation pressure 7Mpa, temperature 40 ° C; separation kettle 2 separation pressure 5Mpa, temperature 35 ° C to separate the maca fat-soluble active substance, and collect the maca extract residue;

[0027] , feed intake according to the solid-liquid ratio of maca extract residue and h...

Embodiment 2

[0030] Select fresh and high-quality maca rhizomes from Lijiang, Yunnan, place them in a vacuum drying room, and vacuum-dry them at a vacuum degree of 0.07Mpa and a temperature of 50°C until the moisture content is 6%; use liquid nitrogen low temperature pure physical wall breaking technology to break the wall After sieving treatment, the broken wall particle size is 200 mesh, and the dry maca powder is granulated by alcohol wet method, and the particle size is 20 mesh. Weigh 9 kg of maca granules and put them into the extraction container. C, CO 2Extract at a flow rate of 25L / hr for 2 hours, then feed in 7% edible 95% ethanol as a carrier, and extract for another 1 hour. Separation pressure 9Mpa through separation kettle 1, temperature 50 DEG C; separation kettle 2 separation pressure 6Mpa, temperature 45 DEG C to separate the maca fat-soluble active substance, and collect the maca extract residue;

[0031] , feed intake according to the solid-liquid ratio of maca extract re...

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Abstract

The invention discloses a method for extracting an active ingredient from maca. The method comprises the following steps of: performing vacuum drying on roots and stalks of the maca which are taken as a raw material, breaking walls, crushing, performing wet granulation, performing supercritical carbon dioxide extraction, separating to obtain a fat-soluble active substance in the maca, and extracting maca polysaccharide from maca extract residue by a hot water extraction method. According to the method, a functional active factor in the maca is extracted by a supercritical carbon dioxide extraction technology, and then the maca polysaccharide in the extract residue is extracted by the hot water extraction method; and the high-efficiency extraction and comprehensive utilization of the active ingredient in a maca raw material are realized by a separation and screening combination method from a crude extract to an effective part and the active ingredient.

Description

technical field [0001] The invention belongs to the technical field of extraction and purification of natural biological resources, and relates to a method for comprehensively utilizing maca and fully extracting effective components of maca. Background technique [0002] Maca (Maca) botanical name is Lepidium.meyenii Walp, which belongs to Brassicaceae and Lepidium genus. It is an annual herb plant and is a natural medicinal and edible plant. Native to the South American Andes at an altitude of 3500-4500m, it has been planted and eaten in South America for thousands of years. Maca is used in folk medicine to increase energy, improve fertility, relieve menopausal symptoms in postmenopausal women, depression, treat asthma, and promote wound healing, among others. However, due to the limitation of technological development level, the intensive processing level of Maca is low. For a long time, Maca has only been used as a common food or simply processed, such as processed into ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/31C08B37/00A61P11/06A61P17/02A61P15/08A61P15/12A61P25/24A61K125/00A61K135/00
CPCY02P20/54
Inventor 毛日文朱惠芬王健杨琴张林
Owner JIANGSU JIANGDAYUAN ECOLOGICAL BIOLOGICAL TECH
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