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Manufacturing process of lanthanum oxide cerium rare-earth polishing powder

The technology of rare earth polishing powder and lanthanum cerium oxide is applied in rare earth metal compounds, polishing compositions containing abrasives, inorganic chemistry, etc., and can solve the problem that the finished product of lanthanum cerium oxide rare earth polishing powder is irregular in shape and the surface smoothness of the polished body decreases. , lattice arrangement disorder and other problems, to achieve the effect of not easy to deep scratch, shorten the grinding time and improve the surface accuracy

Active Publication Date: 2013-04-03
ANYANG JINSHI ABRASIVE MATERIALS
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the current production process, the reaction time is fast, the crystallization is rapid, and the crystal lattice is disordered, resulting in irregular shape of the finished product of lanthanum cerium oxide rare earth polishing powder. deep scratch

Method used

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  • Manufacturing process of lanthanum oxide cerium rare-earth polishing powder

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Embodiment Construction

[0007] Dissolve rare earth chloride raw materials and alkaline reactants (such as sodium bicarbonate, ammonium bicarbonate, etc.) in industrial pure water, and add acid co-reactants (such as hydrochloric acid, silicon Hydrofluoric acid, sulfuric acid, etc.) to control the pH value of 3.5-4; when dissolving alkaline reagents (such as: ammonium bicarbonate, sodium bicarbonate, etc.), the pure water in the processing industry controls the concentration of alkaline reagents at 10%-35% . The dissolved rare earth raw materials are filtered and added to the parent compound preparation device ∮2000-8.5, heated and stirred with steam, the temperature is controlled between 40°C and 90°C, and the liquid alkaline reactant is added dropwise, and the parent compound is prepared. When the pH value of the reactant in the preparation device ∮2000-8.5 reaches 6--7, the filling of the alkaline reactant is completed; after 4 hours of fluorinated lattice transformation, it is dehydrated by a YZLFH...

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Abstract

The invention discloses a manufacturing process of lanthanum oxide cerium rare-earth polishing powder. The manufacturing process adopts the technical scheme that the manufacturing process comprises the steps that a rare earth chloride raw material is dissolved by water; an acid reaction assistant is added; after the rare earth chloride raw material is dissolved, a filtered solvent is put into a parent compound preparing device to be heated; liquid alkaline reactant is added in a dripping manner; when a certain PH value is reached, adding is completed; fluorinated crystal lattices in the preparing device after being transformed for a certain time are sent to a press filter for dehydration, dryout, calcination and cooling; and then the fluorinated crystal lattices are sieved, smashed, and packaged into a finished product. The manufacture process has the benefits that the process is simple in operation method, good in feasibility, and good in effect. The shape of the polishing powder manufactured with the method can improve the accuracy of a ground surface largely, and does not cause deep scratching; the surface smoothness is high; and the requirement of a large area liquid crystal screen on the smoothness is met.

Description

technical field [0001] The invention relates to a production process for controlling the dissolution of raw materials, the addition of alkaline reactants and acid co-reactants and the reaction time when producing nano-scale lanthanum cerium oxide rare earth polishing powder. technical background [0002] The currently recognized production process is that when the raw material rare earth chloride is dissolved, the pH value is not controlled, and the alkaline reactant (such as: sodium bicarbonate) is added as a solid one-time addition, and the reaction temperature is controlled at 30°C-- 45°C, when the pH value in the parent compound preparation device reaches 6.5-7, the reaction ends, and after the reaction is completed, it is directly dehydrated and dried. However, in the current production process, the reaction time is fast, the crystallization is rapid, and the crystal lattice is disordered, resulting in irregular shape of the finished product of lanthanum cerium oxide ra...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01F17/00C09G1/02
Inventor 张海水
Owner ANYANG JINSHI ABRASIVE MATERIALS
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