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High thermal conductivity carbon fiber resin-based composite material and preparation method thereof

A composite material and carbon fiber technology, which is applied in the field of high thermal conductivity carbon fiber resin-based composite materials and their preparation, can solve the problems of low thermal conductivity at room temperature and the like, and achieve the effects of simple preparation process, wide application field and good repeatability

Inactive Publication Date: 2013-05-01
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, new heat-conducting materials made of these traditional heat-conducting substances as heat-conducting fillers compounded with polymer resins or plastics have been widely used, such as "a polymer heat-conducting composite material and its preparation method" (CN10192489A), "a kind of Long carbon fiber reinforced high thermal conductivity polymer composite material and its preparation method” (CN102477182A), “high thermal conductivity plastic and its preparation method” (CN201110137817X) and “a thermal conductivity plastic and its preparation method” (CN102746560A) and other patent technologies, but the above The room temperature thermal conductivity of the materials prepared by the technology is generally low, only 2~10W / m·K

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A high thermal conductivity carbon fiber resin-based composite material and a preparation method thereof. The mesophase pitch-based carbon fiber is used as the thermal conductivity enhancing material, the polymer resin is used as the matrix material, and the volume filling rate of the mesophase pitch-based carbon fiber is 10-30%.

[0021] Firstly, the polymer resin is evenly coated on the surface of the mesophase pitch-based carbon fiber filaments, then laid in one direction in the mold, and then poured to form a high thermal conductivity carbon fiber resin-based composite material.

[0022] In this embodiment: the cross-sectional shape of the mesophase pitch-based carbon fiber is circular; the polymer resin is a solution of ABS resin dissolved in acetone, and the mass ratio of ABS resin to acetone is 1: (4~5) ; The coating method is dipping; the temperature of the casting molding is 50~80 o C, the time is 10~24h.

Embodiment 2

[0024] A high thermal conductivity carbon fiber resin-based composite material and a preparation method thereof. The mesophase pitch-based carbon fiber is used as the thermal conductivity enhancing material, the polymer resin is used as the matrix material, and the volume filling rate of the mesophase pitch-based carbon fiber is 20-50%.

[0025] Firstly, the polymer resin is evenly coated on the surface of the mesophase pitch-based carbon fiber filaments, and then cross-arranged in the mold, and then poured to form a high thermal conductivity carbon fiber resin-based composite material.

[0026] In this embodiment: the cross-sectional shape of the mesophase pitch-based carbon fiber is strip-shaped; the polymer resin is liquid epoxy resin; the coating method is brushing; the casting temperature is 80 ~160 o C, the time is 5~15h.

Embodiment 3

[0028] A high thermal conductivity carbon fiber resin-based composite material and a preparation method thereof. The mesophase pitch-based carbon fiber is used as the thermal conductivity enhancing material, the polymer resin is used as the matrix material, and the volume filling rate of the mesophase pitch-based carbon fiber is 25-60%.

[0029] Firstly, the polymer resin is evenly coated on the surface of the mesophase pitch-based carbon fiber filaments, then laid in one direction in the mold, and then poured to form a high thermal conductivity carbon fiber resin-based composite material.

[0030] In this embodiment: the cross-sectional shape of the mesophase pitch-based carbon fiber is circular; the polymer resin is liquid phenolic resin; the coating method is spraying; the casting temperature is 150-200 o C, the time is 3~8h.

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Abstract

The invention relates to a high thermal conductivity carbon fiber resin-based composite material and a preparation method thereof. According to the technical scheme, intermediate phase pitch based carbon fibers are taken as a heat conduction reinforcing material, a polymer resin is taken as a substrate material, and the volume packing rate of the intermediate phase pitch based carbon fibers is 10-60 percent. The preparation method comprises the following steps: uniformly coating the polymer resin on surfaces of intermediate phase pitch based carbon fiber filaments; unidirectionally paving or orthogonally paving in a cross shape in a mold; and performing casting moulding or hot press moulding to obtain the high thermal conductivity carbon fiber resin-based composite material. The preparation process is simple and high in repeatability; the internal carbon fibers of the prepared high thermal conductivity carbon fiber resin-based composite material have a high orientation arrangement structure, and the thermal diffusion coefficient and the thermal conductivity along the length direction of the fibers can be controlled in a range of 50-400mm<2> / s and a range of 80-500W / m.k according to the difference of carbon fiber filling amount. Therefore, the product has the characteristics of high orientation and high thermal conductivity, and the electrical and mechanical properties along the axial direction of the fibers can be obviously improved.

Description

technical field [0001] The invention belongs to the technical field of resin-based composite materials. In particular, it relates to a high thermal conductivity carbon fiber resin-based composite material and a preparation method thereof. Background technique [0002] In the field of microelectronics technology, due to the increasing integration of electronic circuits, the accumulation of heat will lead to an increase in the temperature of the device, resulting in a decrease in operating stability. According to statistics, every time the temperature of electronic components rises by 2 o C, the reliability drops by 10%, and the temperature rises by 50 o The lifetime of C is only a 25% increase in temperature o 1 / 6 of C life. Therefore, in order to ensure the normal operation of electronic components with high reliability for a long time, the heat conduction and heat dissipation capabilities of materials become important limiting factors affecting their service life. [0...

Claims

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Application Information

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IPC IPC(8): C08L55/02C08L63/00C08L61/06C08K7/06C08K3/04
Inventor 李轩科袁观明易静董志军
Owner WUHAN UNIV OF SCI & TECH
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