Method for controlling secondary stickies through lipase
A technology of lipase and sticky matter, which is applied in the field of waste paper pulping and papermaking, and achieves the effects of low production cost, good effect and simple operation
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Embodiment 1
[0034] Control of secondary stickies in waste paper pulp production using lipase.
[0035] Take 30g of DIP and OCC dry pulp respectively, dilute the pulp with a concentration of 3%, and treat the old newsprint DIP pulp and OCC pulp under different lipase additions. The lipase activity is 20000U / mL, and the pH value is 8.0. The hydrolysis rate of triglyceride is greater than 96%, the rate of lipase transesterification and lipid synthesis is less than 2%, the addition amount is 0.001-0.5% of the weight of DIP and OCC dry pulp respectively, the temperature is 20-60°C, and the time is 60- 120min.
[0036]According to the document Sarja T, Zabihian M and Kourunen P. Control of Potential Secondary Stickies in Deinked Pulp. 2003 TAPPI Fall Technical Conference, Paper 22-2., when the pH of the water sample decreases, the resin and other dissolved The turbidity value of the system increases, and the turbidity difference is the change value between the turbidity and the initial turbidi...
Embodiment 2
[0044] Using lipase to control secondary stickies in papermaking white water.
[0045] 200mL old newsprint DIP pulp and OCC pulp machine white water samples were taken respectively, and treated with different lipase additions. The lipase activity is 20000U / mL, the pH value is 8.0, the addition amount is 0.001-0.5% of the weight of the DIP and OCC pulp machine white water samples, the temperature is 20-60°C, and the time is 60-120min.
[0046] Centrifuge the treated white water of the paper machine at 2000r / min for 15 minutes to remove fine fibers and other components; test the cation demand and turbidity of the centrifuged white water, then use sulfuric acid to adjust the pH to 4, then measure the turbidity, and calculate the pH before and after adjustment difference in turbidity. The test results when the enzyme dosage is 0.001%, 0.05%, and 0.5% are as follows, and the removal rate of secondary stickies is calculated by the change of turbidity difference.
[0047] The resul...
Embodiment 3
[0054] Control of secondary stickies in mechanical pulp production using lipase.
[0055] Take 30g of absolute-dried masson pine TMP slurry, dilute the slurry with a concentration of 3%, and treat the slurry with different amounts of lipase added. The hydrolysis rate is greater than 96%, the lipase transesterification and lipid synthesis rate are less than 2%, the addition amount is 0.001-0.5% of the weight of dry masson pine TMP pulp, the temperature is 20-60°C, and the time is 60-120min.
[0056] Filter the treated slurry, take the filtrate and centrifuge at 2000r / min for 15min to remove components such as fine fibers; test the cation demand and turbidity of the water sample after centrifugation, and then use sulfuric acid to adjust the pH to 4 before measuring the turbidity and calculating Turbidity difference before and after pH adjustment. The test results when the enzyme dosage is 0.001%, 0.05%, and 0.5% are as follows, and the removal rate of secondary stickies is calc...
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