Rapid detection method of contents of multiple components in Chinese patent medicinal traumatic injury treatment tablet
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A detection method and technology of Dieda tablets, which are applied in the directions of measuring devices, material separation, and material analysis, can solve the problems of poor quality controllability of Dieda tablets and the inability to comprehensively and effectively measure the quality of Dieda tablets, and achieve Avoid wasting time and reagents, control quality, and the effect of easy operation of the method
Inactive Publication Date: 2014-07-09
青岛市药品检验所
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Its detection has poor controllability to the quality of Dieda Tablets, and cannot comprehensively and effectively measure the quality of Dieda Tablets.
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[0021] The present invention adopts: instruments and reagents: Shimadzu LC-20AT high performance liquid chromatography; Alltech ELSD2000ES evaporative light scattering detector; Sartoris BP211D electronic balance; acetonitrile is a reagent for chromatography, and other reagents are analytically pure; China National Institutes for Food and Drug Control, batch number: 110736-201136), naringin reference substance (National Institute for Food and Drug Control, batch number: 110722-201111), hesperidin reference substance (National Institute for Food and Drug Control, batch number: 110721 -200613), neohesperidin reference substance (National Institute for Food and Drug Control, batch number: 111857-201102), notoginseng saponin R 1 Reference substance (National Institute for Food and Drug Control, batch number: 110745-200617), ginsenoside Rg 1 Reference substance (National Institute for Food and Drug Control, batch number: 110703-201027), ...
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Abstract
The invention relates to a rapid detection method of multiple components in a Chinese patent medicinal traumatic injury treatment tablet. The contents of eight components comprising paeoniflorin, naringin, hesperidin, neohesperidin, notoginsenoside R1, ginsenoside Rg1, asperosaponin VI and ginsenoside Rb1 in the monarch medicine Himalayan Teasel Root, the minister medicine Panax Notoginseng and the assistant medicines comprising white peony root, Radix Paeoniae Rubra, Cortex Moutan, Immature Bitter Orange and Rhizoma Drynariae of the Chinese patent medicinal traumatic injury treatment tablet are simultaneously determined through the ultrasonic extraction by using methanol, and applying HPLC-ELSD. The rapid detection method solves a problem of many eight-component extraction and determination interferences caused by the large composition and complex components of the traumatic injury treatment tablet, and also avoids the problems comprising time and reagent consumption generated in the multi-time detection needed by the eight components, and inaccurate quantitative detection. The method is simple to operate, substantially improves the working efficiency and the working precision, and is expected to be a standard method for the quality control of the Chinese patent medicinal traumatic injury treatment tablet.
Description
technical field [0001] The invention relates to the field of quality detection of traditional Chinese medicines, in particular to a rapid detection method for multi-component content of Chinese patent medicines in Dieda Tablets. Background technique [0002] Dieda tablets are composed of notoginseng, angelica, white peony root, red peony root, peach kernel, safflower, dried blood, northern liu jinu, rhizome drynaria, diaphan, sumac, peony bark, frankincense, myrrh, turmeric, three It is a large prescription Chinese medicine preparation composed of 24 traditional Chinese medicine decoction pieces including ribs, wind, melon seeds, citrus aurantium, bellflower, licorice paste, Guan Mutong, natural copper, and wood beetle. The main effect is to promote blood circulation and remove blood stasis, reduce swelling and relieve pain. Used for bruises, broken tendons and fractures, blood stasis, swelling and pain, flashes of waist and qi. Its preparation method is to grind Panax not...
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